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Method and equipment for preparing nano grade biological powder material

A nano-scale powder, nano-scale technology, applied in grain processing and other directions, can solve the problems of uneven particle size distribution, unsatisfactory product stability, low product purity, etc., achieving large specific surface area and high energy utilization rate. , the effect of improving solubility

Inactive Publication Date: 2005-11-30
西安邦肽实业有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In recent years, the micronization technology of traditional Chinese medicine has been developed, which uses physical ultrafine pulverization technology to make the medicinal material fineness reach micron or nanometer level. The products obtained by this technology have low purity and uneven particle size distribution, and most of them are targeted at For a single medicinal material, the nanoscale particles are basically above 700 nanometers, and the product stability is not very ideal

Method used

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  • Method and equipment for preparing nano grade biological powder material
  • Method and equipment for preparing nano grade biological powder material

Examples

Experimental program
Comparison scheme
Effect test

specific example 1

[0044] Preparation of nano-scale powder raw materials of Liuwei Dihuang (pills, tablets).

[0045] Ingredients: Yam, Poria, Cornus officinalis, Alisma, Rehmannia glutinosa, Atractylodes macrocephala

[0046] 1. Liquid preparation:

[0047] 1. Soaking:

[0048] Equipment used: heatable microwave multifunctional extraction tank

[0049] Put the medicinal materials in the extraction tank, add the prepared 70-75% solvent ethanol into the extraction tank, completely immerse the raw materials, supply heat, heat the temperature in the tank to 50----60°C, and the pressure in the tank must not exceed 0.02Mpa. Turn off the heat and let stand for 12-14 hours.

[0050] 2. Extraction:

[0051] Equipment used: heatable microwave multifunctional extraction tank

[0052] Stand still for a specified time, supply heat, heat the temperature in the tank to 50--60°C, turn on the circulation pump and microwave generator, and circulate and extract for 10 minutes under heat preservation, then clos...

specific example 2

[0069] Preparation of nanoscale powder of Ganoderma lucidum:

[0070] 1. Liquid preparation:

[0071] 1. Soaking:

[0072] Equipment used: heatable microwave multifunctional extraction tank

[0073] Add drinking water to the extraction tank, submerge the raw materials completely, supply heat, heat the temperature inside the tank to 50----60°C, the pressure inside the tank should not exceed 0.02Mpa, turn off the heat supply, and let it stand for 12-14 hours.

[0074] 2. Extraction:

[0075] Equipment used: heatable microwave multifunctional extraction tank

[0076] Stand still for a specified time, supply heat, heat the temperature in the tank to 50--60°C, turn on the circulation pump and microwave generator, and circulate and extract for 10 minutes under heat preservation, then close the steam valve and continue heat preservation and extraction for 50 minutes , the pressure in the tank shall not exceed 0.02Mpa, turn off the microwave generator and circulation pump, dischar...

specific example 3

[0092] Preparation of Nanoscale Pearl Powder

[0093] 1. Liquid preparation:

[0094] 1. Dissolving:

[0095] Equipment used: heatable microwave multifunctional extraction tank

[0096] Add the prepared aqueous solution with a pH value of 3 into the extraction tank, completely immerse the raw materials, turn on the microwave generator, make it move at a speed of 2-3 billion times / second, and shake and dissolve until the raw materials are completely dissolved into a uniform liquid .

[0097] 2. Concentration:

[0098] Equipment used: low temperature decompression vacuum thin film evaporation concentration equipment

[0099] After transferring the completely dissolved liquid to about 100L in the evaporator, turn on the vacuum pump, start the vacuum system, open the steam valve, and start to concentrate. Control the steam flow rate to keep the temperature at 60±5°C. During the concentration process, the high-concentration and low-concentration ethanol are respectively sent ...

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Abstract

This invention relates to preparation method and equipment for nano-level biological-power raw material which comprises, employing microwave to assist abstraction of continual flow liquid at low temperature, condensing thin membrane and decompressing, and carrying out low temperature supersonic jet spray drying; fit to large range material, and can make obtain needed constituent activity with no damage.

Description

1. Technical field: [0001] The invention relates to preparing nano-scale biological powder from single animal and plant raw materials, multiple compound animal and plant raw materials, single or compound Chinese medicinal materials and Chinese herbal medicine slice raw materials, liquid biological raw materials and hydrolyzable mineral raw materials prepared by appropriate methods body method. 2. Background technology: [0002] In the prior art, traditional methods for preparing traditional Chinese medicine or other plant extract powders are mostly decoction under normal pressure, percolation extraction, normal pressure or reduced pressure concentration, normal pressure and reduced pressure drying, etc. dry or spray dry. Including 3 basic unit processes: (1) Boiling the raw material or reflux extraction at normal temperature; (2) Heating and boiling concentration under normal pressure or boiling concentration under reduced pressure; (3) Static drying under normal pressure o...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B02C19/06
Inventor 王文庚张亚丽
Owner 西安邦肽实业有限公司
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