Functional viscose fiber containing Chinese medicinal component and its preparation method
A viscose fiber, traditional Chinese medicine technology, applied in the direction of rayon made of viscose, etc., can solve problems such as application, limitation of functional fibers of traditional Chinese medicine, harmful radiation pollution, etc.
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Embodiment 1
[0031] Weigh the traditional Chinese medicine honeysuckle to remove impurities, cut, pulverize, rub, and screen to obtain 2 kg of crude honeysuckle with a length of less than 5 mm and mix them with 20 kg of cotton pulp into an impregnation barrel for impregnation. The process conditions are as follows: the concentration of caustic soda for one impregnation is 240g / l, the temperature is 55°C, the time is 50 minutes, the concentration of porridge is 4%, and 1% of impregnation aid LV-3 is added. Carry out secondary impregnation through pressing and pulverizing process, caustic soda concentration is 170g / l, temperature is 45 ℃, time is 30 minutes, and the concentration of porridge is 3.5%. After pressing, the alkali fiber contains 30% of methyl fiber and 14.4% of alkali. After 4 hours of aging, the viscosity of alkali cellulose cupro ammonia reaches 0.0055Pa.s, and the yellowing process parameter CS 2The addition coefficient is 36%, the initial temperature is 18°C, the final temp...
Embodiment 2
[0033] Take 0.5 kg of the screened Acanthopanax senticosus dry powder, mix with 30 kg of alkali cellulose with a methylcellulose content of 30%, and blend to make glue. Yellowing process parameter CS 2 The addition coefficient is 34%, the initial temperature is 21°C, the final temperature is 29°C, the time is 80 minutes, and the wet method is used for yellowing. Dissolved at 17-18°C for 150 minutes, filtered through three times, defoamed and matured for 8 hours. The spinning conditions are that the aperture of the spinneret is 0.06, the spinning speed is 40 m / min, the viscose index is: 8.7% of cellulose, 5.7% of alkali, 33 seconds of viscosity, and 12 ml of maturity. Spinning and drawing process parameters are: acid bath sulfuric acid concentration 133g / l, temperature 48°C, zinc sulfate content 9g / l, sodium sulfate content 335g / l, draw ratio 2.32, plasticizing bath temperature 85-99°C. Post-treatment is carried out after cutting, and the post-treatment process parameters are...
Embodiment 3
[0035] Take the crushed and ground tomato juice, filter it with a 100-mesh steel mesh, take 0.5 kg of its juice, add it to 50 L of primary dissolving viscose and mix it, dissolve and grind it at 20°C for 160 minutes to obtain dissolving glue. After three times of filtration, degassing and aging for 15 hours. The spinning conditions are that the aperture of the spinneret is 0.06, the spinning speed is 45 m / min, the viscose index is: 8.7% of cellulose, 5.5% of alkali, 35 seconds of viscosity, and 9.5ml of maturity. Spinning and drawing process parameters are: acid bath sulfuric acid concentration 125g / l, temperature 50°C, zinc sulfate content 12g / l, sodium sulfate content 325g / l, draw ratio 2.26, plasticizing bath temperature 80-98°C. Post-treatment after cutting, the post-treatment process parameters are: first washing temperature 35°C, alkali content in desulfurization bath 6.5g / l, temperature 78°C, second washing temperature 50°C, third washing temperature 70°C, oil bath conc...
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