Gallium oxide gas sensing film doped with metal oxide and preparation method thereof
A technology of sensing film and gallium oxide, which is applied to the field of gallium oxide gas sensing film doped with metal oxide and its preparation field, can solve the problems of poor gas sensing performance, reduced effective contact area, large particle size, etc. Induction performance, the effect of increasing the effective contact area
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Embodiment 1
[0015] Under nitrogen protection, mix gallium acetylacetonate and tungsten ethoxide in a methanol solvent at a molar ratio of 1:0.05, add deionized water and hydrochloric acid, control the pH value to 2.0, stir for 4 hours, and obtain a coating sol after standing;
[0016] The above-mentioned coating sol was rotated in a homogenizer to coat the film. The speed of the homogenizer was 1600 rpm, the homogenization time was 30s, and the coating was repeated 20 times to obtain a gel film. The obtained gel film was first dried at 240°C for 1 hour, and then dried at 900°C for 1 hour to obtain the product. In the obtained film: the molar content of gallium oxide was 95%, and the average grain size of the film was 23 nm.
Embodiment 2
[0018] Under nitrogen protection, mix gallium acetylacetonate and tungsten ethoxide in a butanol solvent at a molar ratio of 1:0.25, add deionized water and nitric acid, control the pH value to 5.0, stir for 6 hours, and obtain a coating sol after standing still ;
[0019] The above coating sol was rotated in a homogenizer to coat the film. The speed of the homogenizer was 2000 rpm, the homogenization time was 45s, and the coating was repeated 20 times to obtain a gel film. The obtained gel film was first dried at 120°C for 2 hours, and then dried at 800°C for 1 hour to obtain the product. In the obtained film: the molar content of gallium oxide was 80%, and the average grain size of the film was 46 nm.
Embodiment 3
[0021] Under nitrogen protection, mix gallium acetylacetonate and tungsten ethoxide in ethylene glycol at a molar ratio of 1:0.11, add deionized water and sulfuric acid, control the pH value to 3.0, stir for 6 hours, and obtain a coating sol after standing still ;
[0022] The above-mentioned coating sol was rotated in a homogenizer to coat the film. The speed of the homogenizer was 4000 rpm, the homogenization time was 60s, and the coating was repeated 30 times to obtain a gel film. The obtained gel film was first dried at 240°C for 1 hour, and then dried at 800°C for 1 hour to obtain the product. In the obtained film: the molar content of gallium oxide was 90%, and the average grain size of the film was 32 nm.
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