Negative nano-imprinting method
A nano-imprinting and negative-type technology, which is applied in the manufacture of electrical components, semiconductor/solid-state devices, circuits, etc., can solve problems such as easy-to-produce defects, and achieve the effects of easy control, avoiding stripping process, and low price
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Example Embodiment
[0032] Example 1: A negative nanoimprint method, characterized in that it is composed of the following steps (see figure 2 ): (1) First, the metal film layer I5 is vapor-deposited on the silicon substrate 1, and the photoresist 2 is spin-coated on the metal film layer I5 (see figure 2 -a); (2) Then copy the nano pattern of template 3 to photoresist 2 under heating and pressurizing conditions (see figure 2 -b), (3) and use reactive ion etching technology to transfer the pattern to the metal-plated layer I5 (see figure 2 -c); (4) Then use the pattern of photoresist 2 as a mask to etch the bare metal I5 that is not covered by photoresist 2 by wet chemical etching (see figure 2 -d); (5) Metal nanostructures are prepared.
[0033]The metal nanostructure prepared in the above step (5) is directly dissolved in the photoresist 2 in an organic solvent to obtain a single metal nanostructure (see figure 2 -e).
Example Embodiment
[0034] Embodiment 2: A negative nanoimprint method, characterized in that it is composed of the following steps (see figure 2 ): (1) First, the metal film layer I5 is vapor-deposited on the silicon substrate 1, and the photoresist 2 is spin-coated on the metal film layer I5 (see figure 2 -a); (2) Then copy the nano pattern of template 3 to photoresist 2 under heating and pressurizing conditions (see figure 2 -b), (3) and use reactive ion etching technology to transfer the pattern to the metal-plated layer I5 (see figure 2 -c); (4) Then use the pattern of photoresist 2 as a mask to etch the bare metal I5 that is not covered by photoresist 2 by wet chemical etching (see figure 2 -d); (5) Metal nanostructures are prepared.
[0035] The metal nanostructures produced in the above step (5) are vapor-deposited metal II6 using the pattern of photoresist 2 as a mask (see figure 2 -f), and then remove the photoresist 2 with an organic solvent to prepare bimetallic nanostructures (see ...
Example Embodiment
[0036] Example 3: Preparation of SiO by combining direct-write electrical beam exposure technology and reactive ion etching technology 2 / Si template, the line width, period and height of the template pattern are 170nm, 370nm and 130nm respectively. Take a 2×2cm silicon wafer, evaporate a 25nm thick gold film after cleaning, then spin-coat photoresist on the surface of the gold film, and dry it at 170°C to a thickness of 150nm, and then copy the nano-patterns on the template to the On photoresist (imprinting conditions: 190°C, 45bar, 3min). The reactive ion etching process is used to remove the excess photoresist in the trench, and the nano-pattern is transferred to the surface of the gold film. Then use the photoresist nano-pattern as a mask, and use KI / I 2 Solution (0.0025M I 2 +0.015M KI) dissolve the exposed gold film for 40 seconds, and then remove the photoresist with hot acetone under ultrasonic conditions to obtain a gold nanostructure with a line width of 400nm. Such as i...
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