Process for synthesizing organometallic antimonide
A synthesis process and organometallic technology, applied in the direction of antimony organic compounds, etc., can solve the problems of increasing cost and investment, reducing the conversion rate of antimony trioxide, and low activity
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0028] In a four-necked 500M1 flask with a stirrer, thermometer, and rectification tube (connected to a vacuum pump and hydrogen and nitrogen lines) that can be heated, add 50 grams of antimony trioxide (purity 99.8%) and 200 grams of ethylene glycol (purity) 99.5%). Start the vacuum pump. When the pressure of the vacuum gauge is -0.09MPa, stop the pump and slowly turn on the nitrogen to make the pressure zero. Repeat the operation three times to replace the oxygen in the bottle as much as possible. Then open the hydrogen or the mixed gas valve of hydrogen and nitrogen to enter the gas, make the pressure -0.05MPa, heat under stirring, control the temperature at 160-170°C, and react for 120 minutes. During the heating reaction process, the pressure is maintained at -0.06MPa~0.02MPa by supplementing hydrogen and nitrogen, and the water and other substances generated by the reaction are separated through the rectification tube, and no water is discharged, and the reaction is complete...
Embodiment 2
[0030] Repeat the operation of Example 1, wherein 50 grams of antimony trichloride and 180 grams of ethylene glycol are added. After 120 minutes of reaction, the reaction solution was transparent and colorless. The vacuum was released with nitrogen, cooled to room temperature under stirring, separated and dried to obtain white crystals of antimony glycol, with an antimony content of 57.35%.
Embodiment 3
[0032] Repeat the operation of Example 1, wherein 50 grams of antimony oxychloride and 250 grams of ethylene glycol are added. After 120 minutes of reaction, the reaction solution was transparent and colorless. The vacuum was released with nitrogen, cooled to room temperature under stirring, and separated and dried to obtain white crystals of antimony glycol with antimony content of 57.4%.
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com