The invention relates to a method using
antimony oxide to produce
sodium antimonate. The method includes: heating the
antimony oxide for 20 minutes, adding into a reactor container, adding
hydrochloric acid and water, adding
sodium polyacrylate while stirring, adding
sodium hydroxide into the reaction container, continuing stirring, controlling
reaction temperature to be 50-60 DEG C to perform reaction for 30-40 minutes, and feeding
oxygen into the reaction container; slowly adding
hydrogen peroxide, controlling
reaction temperature to be 40-50 DEG C, and continuing performing reaction for 10 minutes after the adding of the
hydrogen peroxide is completed in 30-50 minutes, and stopping stirring; standing, cooling to
room temperature to filter out precipitates, washing the precipitates with water, and
drying the washed precipitates until the
moisture of the precipitates is smaller than 0.3% to obtain the
sodium antimonate. By the method, the conversion of the
antimony oxide during reaction is promoted, conversion rate is increased, and accordingly the production efficiency of the
sodium antimonate is increased,
raw material utilization rate is increased, the production time of the
sodium antimonate is lowered effectively, and
raw material use amount is reduced.