Flow regulated pressure swing adsorption system

a pressure swing and adsorption technology, applied in the field of separation, can solve the problems of inability to mechanically immobilize the adsorbent bed, inability to achieve rotary adsorbent bed assembly, and complicated valve logic and control

Inactive Publication Date: 2004-04-13
AIR PROD & CHEM INC
View PDF148 Cites 81 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

The present invention achieves pressurization and depressurization steps primarily by gas exchanges between the adsorbent beds. Steps entailing exchange of gas enriched in the second component between adsorbent beds will be described as light reflux steps. A predetermined logical sequence of ...

Problems solved by technology

With a greater number of beds, multiple pressure equalization steps can be achieved, although the valve logic and controls are then greatly complicated.
For large industrial PSA systems, mechanical immobilization of the adsorbent beds has not been practicable.
However, a rotary adsorbent bed assembly may be impracticable for large PSA units, owing to the weight of the rotating assembly.
Also, when separating gas components which are highly inflammable or toxic, the rotary adsorbent bed assembly would need to be completely enclosed in a containment shroud to capture any leakage from large diameter rotary seals.
However, these prior art devices have limited utility except in small scale applications, owing to their lack of control flexibility.
Since valve timing logic and port orifice sizing of the multiport valves are fixed rigidly in these prior art inventions, there is no provision for flow control to provide operational adjustment under changing feed conditions or during intervals of reduced product demand, or for performance optimization.
This inflexibility of control is most limiting for those of the cited prior art inventions which use multiport valves to exchange gas between a pair of beds, and across a pressure difference between that pair of beds.
Once the internal orifice apertures of the rotary valves and piping connections have been fixed, the prior art PSA cycle using multiport valves could only operat...

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Flow regulated pressure swing adsorption system
  • Flow regulated pressure swing adsorption system
  • Flow regulated pressure swing adsorption system

Examples

Experimental program
Comparison scheme
Effect test

embodiment 1

FIG. 10 is a schematic drawing of an alternative second distributor valve 400 with control means for the adjustable orifices of the rotor as configured for embodiment 1 of FIG. 1. Adjustable orifices 96-98 are provided as throttle valves mounted in rotor 80, each with identical or similar external actuation means, described here in detail for adjustable orifice 97. Light reflux withdrawal port 91 communicates by conduit 401 to upstream valve chamber 402. Chamber 402 is penetrated by valve stem 405 with coaxial needle 406 aligned with valve seat 408. The adjustable throttle valve orifice is defined between needle 406 and seat 408, and provides fluid communication with downstream valve chamber 410 which in turn communicates by conduit 412 to light reflux return port 94.

Drive end 414 of valve stem 405 is isolated from process fluid by seal 415, and is provided with a drive pin 416 penetrating a drive slot 417 in rotor 80. Slot 417 has axial clearance for pin 416, sufficient for movemen...

embodiment 450

An alternative embodiment 450 of the second distributor valve uses fluid transfer chambers between the rotor 80 and the stator housing 78, so that the adjustable orifices can be provided as throttle valves external to the stator housing.

On a common sealing diameter, rotary seals 451, 452, 453, 454 and 455 mutually isolate chamber 107 communicating in rotor 80 to light reflux withdrawal port 90 at substantially the higher pressure, transfer chamber 461 communicating to light reflux return port 93, transfer chamber 462 communicating to light reflux withdrawal port 91, transfer chamber 463 communicating to light reflux return port 94, transfer chamber 464 communicating to light reflux withdrawal port 92, and chamber 109 communicating to light reflux return port 95 at substantially the lower pressure. Adjustable orifice 96 is provided as throttle valve 471 communicating through stator housing 78 to chambers 107 and 461. Adjustable orifice 97 is provided as throttle valve 472 communicati...

embodiment 600

of the first distributor valve is energized by the externally imposed pressure difference between the higher pressure in conduit 126 and the lower pressure in conduit 121. The axial thrust load exerted by the ring of annular pistons approximately balances the pressure distribution on the valve surface, so that excessively high contact pressures can be avoided.

FIG. 15

Another embodiment 700 of the distributor valves, here illustrated for a first distributor valve, uses a single eccentric loading device to achieve approximate radial balance of the rotor, while balancing the stator using loading pistons analogous to those used in the rotor of embodiment 600. Components common to first distributor valve 37 of FIG. 1 are denoted with equivalent reference numerals.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

PropertyMeasurementUnit
Timeaaaaaaaaaa
Forceaaaaaaaaaa
Pressureaaaaaaaaaa
Login to view more

Abstract

Pressure swing adsorption (PSA) separation of a gas mixture is performed in an apparatus with a plurality of adsorbent beds. The invention provides rotary multiport distributor valves to control the timing sequence of the PSA cycle steps between the beds, with flow controls cooperating with the rotary distributor valves to control the volume rates of gas flows to and from the adsorbent beds in blowdown, purge, equalization and repressurization steps.

Description

TECHNICAL FIELDThe invention relates to separations conducted by pressure swing adsorption (PSA). The present invention provides simplified controls, with enhanced flexibility of control adjustment through flow regulation under changing operating conditions.BACKGROUND ARTGas separation by pressure swing adsorption is achieved by coordinated pressure cycling and flow reversals over adsorbent beds which preferentially adsorb a more readily adsorbed component relative to a less readily adsorbed component of the mixture. The total pressure is elevated to a higher pressure during intervals of flow in a first direction through the adsorbent bed, and is reduced to a lower pressure during intervals of flow in the reverse direction. As the cycle is repeated, the less readily adsorbed or "light" component is concentrated in the first direction, while the more readily adsorbed or "heavy" component is concentrated in the reverse direction.The conventional process for gas separation by pressure ...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
IPC IPC(8): B01D53/047B01D53/04
CPCB01D53/0446B01D53/047B01D2253/108B01D2253/25B01D2256/16B01D2257/504B01D2258/0208B01D2259/40005B01D2259/4003B01D2259/40037B01D2259/40067B01D2259/4062Y10T137/86863Y02C20/40
Inventor KEEFER, BOWIE G.DOMAN, DAVID G.
Owner AIR PROD & CHEM INC
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products