The invention discloses a method for preparing regular petal-shaped WO3/Fe2O3, and relates to a method for preparing WO3/Fe2O3, which comprises the following steps: by taking hydrazine hydrate, methylbenzene, ferric acetylacetonate, oleic acid and sodium tungstate as main raw materials, adding an acidic solution to adjust the pH value, putting into a reaction kettle at 130 DEG C, taking out the solution after 24 hours, cooling at room temperature, adding ethanol into the obtained product Fe3O4, carrying out ultrasonic treatment, cleaning with ethanol under the help of a magnet, and drying to obtain the regular petal-shaped WO3/Fe2O3. And storing in ethanol for later use. Taking 5 mmol of sodium tungstate, putting the sodium tungstate into a reaction kettle lining, stirring and dissolving, adjusting the pH value to be about 4.5 by using an acid solution, adding Fe3O4 soaked in ethanol, reacting at 160 DEG C for 96 hours, taking out the solution, cooling at room temperature, centrifugally cleaning the obtained product by using deionized water, putting into a drying oven for vacuum drying at 65 DEG C, and grinding the treated solid in an agate mortar to obtain the final product WO3/Fe2O3. The WO3/Fe2O3 prepared by the invention has the characteristics of small size, uniform morphology, high yield, low cost, simple synthesis process, environmental friendliness, no toxicity, excellent chemical stability, magnetism and the like, and has wide application prospects.