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Method for manufacturing high silicon grain-oriented electrical steel sheet with superior core loss property

A technology of grain orientation and electrical steel plate, which is applied in the direction of metal material coating process, coating, solid-state diffusion coating, etc., to achieve the effect of excellent iron loss performance

Inactive Publication Date: 2008-11-05
浦项股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Therefore, various attempts have been made to produce a grain-oriented electrical steel sheet having excellent magnetic properties due to a high silicon content, but no such product has been successfully produced.

Method used

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  • Method for manufacturing high silicon grain-oriented electrical steel sheet with superior core loss property
  • Method for manufacturing high silicon grain-oriented electrical steel sheet with superior core loss property

Examples

Experimental program
Comparison scheme
Effect test

Embodiment approach 1

[0050] Each containing Si: 3.05wt%, C: 0.046wt%, P: 0.015wt%; molten aluminum: 0.026wt%, N: 0.0073wt%, S: 0.005wt%, Mn: 0.11wt%, Cu: 0.12wt% %, with the balance being iron and unavoidable impurities, the slab is reheated at 1190°C, and then hot-rolled, annealed and pickled at a temperature lower than 1190°C. After that, the hot-rolled steel sheet is cold-rolled to obtain a thickness of 0.20-0.30 mm. The 0.20mm thick steel plate was additionally hot-rolled and annealed during rolling to ensure the final cold-rolling ratio. Decarburization annealing was performed on the cold-rolled steel sheet at 880° C. in a humid atmosphere containing nitrogen and hydrogen mixed gas to control the residual carbon content, and at the same time, a decarburization annealed steel sheet with a total surface oxygen content of 610 ppm was obtained.

[0051] Next, an annealing separator was coated on one of the cold-rolled steel sheets obtained above to manufacture a grain-oriented electrical steel s...

Embodiment approach 2

[0061] Each containing Si: 3.20wt%, C: 0.045wt%, P: 0.014wt%; molten aluminum: 0.027wt%, N: 0.0075wt%, S: 0.005wt%, Mn: 0.10wt%, Cu: 0.12wt% %, the balance is iron and unavoidable impurities, the steel billet is reheated at 1150°C, and then hot-rolled, annealed and pickled at a temperature lower than 1100°C. Thereafter, the hot-rolled steel sheet was cold-rolled to obtain a final thickness of 0.23 mm. Then decarburize the cold-rolled steel sheet at an annealing temperature of 880° C. in a humid atmosphere containing nitrogen and hydrogen to obtain a decarburized annealed steel sheet.

[0062] Next, 25 parts by weight of Fe-Si based sintered powder having -325 mesh and containing 50% Si were mixed with 100 parts by weight of MgO, and the mixture was dispersed in water to obtain a slurry siliconized composition. The above siliconized composition was coated on the surface of the decarburized annealed steel sheet with a roll coater. Afterwards, the steel sheets are dried and coi...

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Abstract

There is provided a method for manufacturing a high silicon grain-oriented electrical steel sheet. In a method for manufacturing a high silicon grain-oriented electrical steel sheet, comprising the steps of: reheating and hot-rolling a steel slab to produce a hot-rolled steel sheet; annealing the hot-rolled sheet and cold rolling the annealed steel sheet so as to adjust a thickness of the steel sheet; decarburization annealing the cold rolled steel sheet; and finish-annealing the decarburization annealed steel sheet for secondary recrystallization, the improved method further comprising the step of: coating a powder coating agent for siliconization on a surface of the decarburization annealed steel sheet in a slurry state, the powder coating agent including 100 part by weight of MgO powder and 0.5 - 120 part by weight of sintered powder of Fe-Si compound containing 25 70 wt.% Si sintered powder, the sintered powder having a grain size of -325 mesh; drying the resultant decarburization annealed steel sheet; and finish annealing the steel sheet under a conventional condition.

Description

technical field [0001] The invention relates to a method for manufacturing a high-silicon grain-oriented electrical steel sheet with improved magnetic properties, especially improved iron loss. More specifically, the present invention relates to a method of manufacturing a high-silicon grain-oriented electrical steel sheet, wherein the surface of the steel sheet is coated with a siliconization (siliconization) powder coating agent containing an annealing release agent, and the final annealing is carried out to produce an excellent high-frequency magnetic And electrical steel plate with excellent power frequency performance. Background technique [0002] Generally, electrical steel sheets are divided into grain-oriented electrical steel sheets and non-oriented electrical steel sheets. The grain-oriented electrical steel sheet contains 3% silicon (Si) and has a crystal texture with a grain orientation of {(110)[001]}. Its excellent magnetic properties along the rolling direc...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C21D8/12C23C10/46
CPCC23C10/02C23C10/46
Inventor 崔圭升禹宗秀金在宽
Owner 浦项股份有限公司