Quaternary magnesium base hydrogen storage alloy, its producing method and use
A magnesium-based hydrogen storage alloy and production method technology, applied in the field of materials, can solve problems such as unstable performance, low practicability, and high hydrogen absorption/decomposition temperature
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Embodiment 1
[0015] (1) According to Mg 1.95 Al 0.05 Ni 0.92 V 0.08 Weigh the alloying element powder, mix thoroughly, and then press into flakes; put the pressed flake samples into a vacuum with a degree of 1×10 -3 Sintering in a Pa vacuum sintering furnace, the sintering temperature is 500-800°C, and the sintering time is 1.5-4 hours; then the alloy samples obtained by sintering are crushed, ball milled, and screened to obtain Mg with a particle size below 25μm 1.95 Al 0.05 Ni 0.92 V 0.08 alloy powder;
[0016] (2) Press Mg 1.95 Al 0.05 Ni 0.92 V 0.08 3.5% of the alloy powder weight takes by weighing fine Ni powder and carries out ball milling, observes microstructure with x-ray diffractometer (XRD) in the ball milling process, sees whether to become nanocrystalline Ni powder, usually appears nanocrystalline structure after 15 hours;
[0017] (3) Mg with a particle size below 25 μm 1.95 Al 0.05 Ni 0.92 V 0.08 Alloy powder and nanocrystalline Ni powder and Mg 1.95 Al 0.05...
Embodiment 2
[0020] (1) with embodiment 1;
[0021] (2) Press Mg 1.95 Al 0.05 Ni 0.92 V 0.08 3% of alloy powder weight takes by weighing fine Ni powder and carries out ball milling, and all the other are with embodiment 1;
[0022] (3) Mg with a particle size below 25 μm 1.95 Al 0.05 Ni 0.92 V 0.08 Alloy powder and nanocrystalline Ni powder and Mg 1.95 Al 0.05 Ni 0.92 V 0.08 2-3% TiO by powder weight 2 After fully mixing with 0.1% carbon nanotubes, carry out high-energy ball milling, and the rest are the same as in Example 1.
[0023] The finished product obtained has the following performance indicators after testing: hydrogen storage capacity 3-5.5% (weight percent), hydrogen absorption / decomposition temperature 500, electrochemical capacity 450mA·h·g -1 .
Embodiment 3
[0025] (1) with embodiment 1;
[0026] (2) Press Mg 1.95 Al 0.05 Ni 0.92 V 0.08 5% of alloy powder weight takes by weighing fine Ni powder and carries out ball milling, and all the other are with embodiment 1;
[0027] (3) Mg with a particle size below 25 μm 1.95 Al 0.05 Ni 0.92 V 0.08 Alloy powder and nanocrystalline Ni powder and Mg 1.95 Al 0.05 Ni 0.92 V 0.08 3% TiO by powder weight 2After fully mixing with 1% carbon nanotubes, carry out high-energy ball milling, and the rest are the same as in Example 1.
[0028] The finished product obtained has the following performance indicators after testing: hydrogen storage capacity 3-5.5% (weight percent), hydrogen absorption / decomposition temperature 500, electrochemical capacity 450mA·h·g -1 .
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