Quality control method of bone sinew medicinal pill preparation

A detection method, the technology of Gujin Wan, which is applied in the field of quality control of medicines and Gujin Wan preparations, can solve problems such as backward quality control standards, difficult product quality control, and inability to effectively control the quality of Gujin Wan preparations.

Inactive Publication Date: 2009-07-29
GUIZHOU YIBAI PHARMA CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Among them, "Gujinwan Capsules" and "Gujinwan Tablets" are recorded in the thirteenth volume of traditional Chinese medicine prescriptions issued by the Ministry. This medicine has been used clinically for many years. , proliferative arthritis, Kashin-Beck disease and other diseases have achieved relatively satisfactory therapeutic effects, but our research found that the existing Gujin Wan preparations have the disadvantages of simple and backward quality control standards and difficult product quality control
Since Radix Paeoniae Alba, Panax notoginseng, Corydalis Corydalis, Duhuo, Gentiana chine

Method used

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  • Quality control method of bone sinew medicinal pill preparation
  • Quality control method of bone sinew medicinal pill preparation
  • Quality control method of bone sinew medicinal pill preparation

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0111] Quality control methods for Gujinwan capsules, tablets or granules.

[0112] To observe the traits, the steps are;

[0113] For capsules: the contents are brown; smell, bitter and astringent;

[0114] For tablets; the drug is brown; smell, bitter, astringent;

[0115] For granules: the product is brown granules;

[0116] To identify the contents, the steps are:

[0117] (1) Take capsules, tablets or granules respectively and observe under a microscope: gelatinized starch granules are light yellow or nearly colorless; hypodermal sclerenchyma cells are green and yellow, and the cells are polygonal, square or long. , the wall is slightly curved, lignified, some become beaded and thickened, and the pits are fine; the stone cells are light yellow, sub-round or oblong, with a diameter of about 60 μm, the wall is thicker, and the pits are fine; the diameter of the threaded vessel is 16 ~32μm; many starch granules, single round, semicircular or round polygonal, 4~30μm in di...

Embodiment 2

[0127] To observe the traits, the steps are:

[0128] For capsules: the contents are brown; smell, bitter and astringent;

[0129] For tablets: the drug is brown; the smell is bitter and astringent;

[0130] For granules: the product is brown granules;

[0131] To identify the contents, the steps are:

[0132] (1) Take capsules, tablets or granules respectively and observe under a microscope: gelatinized starch granules are light yellow or nearly colorless; hypodermal sclerenchyma cells are green and yellow, and the cells are polygonal, square or long. , the wall is slightly curved, lignified, some become beaded and thickened, and the pits are fine; the stone cells are light yellow, sub-round or oblong, with a diameter of about 60 μm, the wall is thicker, and the pits are fine; the diameter of the threaded vessel is 16 ~32μm; many starch granules, single round, semicircular or round polygonal, 4~30μm in diameter; compound grains are composed of more than 2~10 sub-grains; re...

Embodiment 3

[0143] To observe the traits, the steps are:

[0144] For capsules: the contents are brown; smell, bitter and astringent;

[0145] For tablets: the drug is brown; the smell is bitter and astringent;

[0146] For granules: the product is brown granules;

[0147] To identify the contents, the steps are:

[0148] (1) Take capsules, tablets or granules respectively and observe under a microscope: gelatinized starch granules are light yellow or nearly colorless; hypodermal sclerenchyma cells are green and yellow, and the cells are polygonal, square or long. , the wall is slightly curved, lignified, some become beaded and thickened, and the pits are fine; the stone cells are light yellow, sub-round or oblong, with a diameter of about 60 μm, the wall is thicker, and the pits are fine; the diameter of the threaded vessel is 16 ~32μm; many starch granules, single round, semicircular or round polygonal, 4~30μm in diameter; compound grains are composed of more than 2~10 sub-grains; re...

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Abstract

The invention relates to a quality control method of Gujin pill preparation. The method uses thin-layer chromatography to identify licorice, motherwort and Xu Changqing, and uses high-performance liquid chromatography to measure the content of glycyrrhizic acid. The quality control method has good precision, sensitivity and stability, ensuring the safety, uniformity, stability, effectiveness and controllability of the product quality.

Description

Technical field: [0001] The invention relates to a quality control method of Gujin Wan preparation, which belongs to the field of pharmaceutical technology. technical background: [0002] Hypertrophic spondylitis, cervical spondylosis is a common disease that endangers the health of people today. [0003] Gujin Wan preparation is composed of frankincense, myrrh, white peony root, corydalis (made from vinegar), notoginseng, woody, safflower, turmeric, solitary life, achyranthes bidentata, gentiana, cassia twig, dried blood, and nux. Composed of fourteen herbs; it has the effects of promoting blood circulation and removing blood stasis, relaxing tendons and collaterals, dispelling wind and relieving pain, and is used to treat hypertrophic spondylitis, cervical spondylosis, heel spurs, hypertrophic arthritis, Kashin-Beck disease and other diseases. Among them, "Gujinwan Capsules" and "Gujinwan Tablets" are recorded in the thirteenth volume of traditional Chinese medicine presc...

Claims

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Application Information

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IPC IPC(8): G01N30/90A61K36/9066A61K36/51A61K36/328A61K36/21A61K9/08A61K9/10A61K9/16A61K9/20A61K9/48A61P19/08G01N30/02G01N33/15
Inventor 叶湘武张梅
Owner GUIZHOU YIBAI PHARMA CO LTD
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