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Alcohol crossed circle manufacturing technique with potatoes as the main materials

A production process, a double-circle technology, applied in biofuels, fermentation, etc., can solve the problems of liquefied enzymes not working normally, not using industrial production scale, and high-concentration wastewater discharge, so as to reduce investment in fixed assets and eliminate inhibition. , to achieve the effect of zero emissions

Active Publication Date: 2009-11-11
JIANGNAN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The main problems of the method of producing biogas by anaerobic fermentation first and then aeration and aerobic treatment are that it occupies a large area and requires high investment; As high as about 20 yuan, the third is that the treatment of wastewater is difficult to complete, and the discharged wastewater COD cr Still around 500mg / L
There is also a process of using distillation waste liquid full-cycle batching, but because the distillation waste mash after alcohol fermentation contains a large amount of organic acids, the pH value is between 3.0 and 4.0, and the liquefaction enzyme cannot function normally when the starchy raw material is liquefied after batching. (The optimal pH value of liquefying enzyme is between 5.5 and 6.5), resulting in high cost, limited circulation batches, and still a large amount of high-concentration wastewater discharge. This method has not been used on an industrial production scale.

Method used

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  • Alcohol crossed circle manufacturing technique with potatoes as the main materials

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] The present invention uses potatoes as the main raw material for the alcohol double ring production process to adopt the following process steps:

[0025] Take 100g of sweet potato powder, add 200ml of the previous batch of anaerobic fermentation digestion liquid, add 0.07ml of high-temperature-resistant α-amylase, stir evenly and heat, keep warm at 95°C for 60 minutes to liquefy; quickly cool down to 58°C, add the previous batch of distillation waste mash 100ml, add 0.15ml of glucoamylase (common commercial glucoamylase) after mixing, keep saccharification at 62°C for 0.5hr, cool down to 30°C after saccharification, add 10% expanded alcoholic yeast, and ferment at constant temperature for 64hr; The volume of the mature fermented liquid is 343ml, and the alcohol concentration is 9.2% (v / v); 32ml (95.2% v / v) of finished alcohol is obtained through distillation and 310ml of distilled waste mash is obtained. Take out 100ml of waste mash as water for the next batch of sacch...

Embodiment 2

[0027] The present invention uses potatoes as the main raw material for the alcohol double ring production process to adopt the following process steps:

[0028] Take 2000g of cassava flour, add 4000ml of the previous batch of anaerobic fermentation digestion liquid, add 1.2ml of high-temperature-resistant α-amylase, stir evenly and heat, keep warm at 95°C for 50 minutes to liquefy; quickly cool down to 62°C, add the previous batch of distillation waste mash 2000ml, add 2.4ml of glucoamylase (common commercial glucoamylase), keep saccharification at 62°C for 0.5hr, cool down to 30°C after saccharification, add 8% expanded alcoholic yeast to ferment at constant temperature, and ferment for 60hr; after fermentation, mature fermentation The liquid volume is 6850ml, and the alcohol concentration is 11.9% (v / v); 740ml (96% v / v) of finished alcohol is obtained through distillation, and 6200ml of distilled waste mash is obtained. Set aside 2000ml of waste mash as water for the next b...

Embodiment 3

[0030] The present invention uses potatoes as the main raw material for the alcohol double ring production process to adopt the following process steps:

[0031] Take 9000kg of cassava flour and add 24m of the last batch of digestive juice 3 , add 3.2 liters of high-temperature-resistant α-amylase, stir evenly and heat, liquefy at 95°C for 60 minutes; quickly cool down to 65°C, add 4m of the previous batch of distilled waste mash 3 , add 9 liters of glucoamylase (common commercial glucoamylase), keep saccharification at 62°C for 0.45hr, cool down to 28°C after saccharification, insert 8% expanded alcoholic yeast for fermentation, and ferment for 66hr; after fermentation, the volume of mature fermentation liquid is 35.6m 3 , the alcohol concentration is 10.3% (v / v); the finished alcohol 3040L (96% v / v) is obtained by distillation, and the distillation waste mash is 32.6m 3 , through the sedimentation tank to separate the mud and sand, leaving 4m 3 The waste mash is used as w...

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Abstract

The invention relates to an alcohol dual manufacturing technique with tuber as the main material in the alcohol fermentation industry technique, which comprises the following steps: mixing starch and the last anaerobic fermentation digestive liquid; heating, liquefying and reducing the temperature by adding maxilase and mixing homogeneously; adding the last distillery slop; saccharifying by adding glucoamylase; reducing the temperature; inoculating the extended culture distillery yeast; culturing in the constant temperature; acquiring the product alcohol by distilling; using distillery slop as the water for the next saccharifying and adjusting acid; cooling the rest slop and inoculating the last activated sludge in order to produce methane with anaerobic fermentation; recovering the activated sludge and digestive liquid by separating anaerobic fermentation liquid; making the digestive liquid back to the proportioning procedure as the technology water; circulating sequentially. The invention only needs a step anaerobic fermentation of distillery slop, which reduces investment of accommodation area and capital assets, can circulate anaerobic fermentation digestive liquid, achieves zero discharge of the wastewater from fermentation, achieves the circulation of the water resource and reduces the cost of alcohol.

Description

technical field [0001] The invention relates to an alcohol double-circle production process using potatoes as the main raw material, and belongs to the technical field of fermented alcohol industry. Background technique [0002] Fermentation of starchy raw materials to produce alcohol is one of the main methods of alcohol production. In the traditional fermentation process of starchy raw materials to produce alcohol, starchy raw materials are crushed, mixed with water, liquefied and saccharified, and then inoculated with alcoholic yeast for fermentation (as introduced in the book "Alcohol Industry Handbook", edited by Zhang Kechang, etc., Light Industry Press ). The traditional fermentation production process averages 12 to 15 tons of waste mash per ton of alcohol, and the waste mash COD cr As high as 40,000-50,000 mg / L or more, it not only causes serious water pollution, but also causes a lot of waste of resources. [0003] The current treatment methods of alcohol produc...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C12P7/06
CPCY02E50/17Y02E50/10
Inventor 毛忠贵张建华
Owner JIANGNAN UNIV
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