Analytical investigating method of perfluor n-pro-pyl vinyl ether
A technology of perfluoro-n-propyl vinyl ether and n-propyl vinyl ether, which is applied in the field of analysis and measurement of perfluoro-n-propyl vinyl ether, can solve the problems of being unsuitable for routine analysis of enterprises and expensive instruments, and achieves The effect of high practical value and simple method
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[0017] Example 1:
[0018] 1.1 Instrument
[0019] Agilent 6890 chromatograph
[0020] 1.2 Chromatographic conditions
[0021] Detector: FID (Flame Ionization Detector)
[0022] Column: DB-17
[0023] Column length: ¢0.25*30m
[0024] Column temperature: 40℃
[0025] Sampler: 120℃
[0026] Detector: 300°C
[0027] 1.3 Sample analysis
[0028] Since the sample is very volatile, be careful to move quickly when injecting the sample. Quickly sample 1uL for chromatographic analysis, and obtain the content of perfluoro-n-propyl vinyl ether by the following formula.
[0029]
[0030] In the formula: A is the peak area of perfluoro n-propyl vinyl ether
[0031] ΣA is the total area of each peak.
[0032] As shown in Figure 1, the peak area of perfluoro-n-propyl vinyl ether is 658020 and the peak area of hydride is 263. Then the content of perfluoro-n-propyl vinyl ether is:
[0033]
[0034] The following is a comparison of the results of nine consecutive determinations of two ...
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[0043] Example 2: Selection of chromatographic conditions
[0044] Install the two groups of DB-1, DB-200, DB-17 with a liquid film of 0.32um and DB-1, DB-200, DB-17 with a liquid film of 1.0um and the aging capillary chromatographic columns respectively. On the Agilent 6890 chromatograph, the resolution test was carried out at different temperatures (column temperature). The results are shown in Table 2 and Table 3. The DB-1, DB-200, and DB-17 are chromatographic column types.
[0045] Table 2 Resolution of a chromatographic column with a liquid film thickness of 1.0um at different temperatures
[0046] Note: Resolution can indicate the separation of each component in the chromatographic column. When the resolution is greater than 1.5, the adjacent two chromatographic peaks can be completely separated. When the resolution is good, the measurement results can have sufficient parallelism and accuracy.
[0047] Table 3 Resolution of the chromatographic column with a liquid film thic...
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