Method for producing rongalite with low zinc
A production method and a technology for carving white blocks, which are applied in chemical instruments and methods, alkali metal sulfites/sulfites, inorganic chemistry, etc., can solve problems such as the inability to meet sodium bisulfite formaldehyde, etc., and achieve improved economic benefits and efficiency. Social benefits, low manufacturing cost, good stability
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Embodiment 1
[0022] The component ratio of the low-zinc carved white block of the present invention is by weight percentage:
[0023] The production method of the low-zinc carved white block of the present invention adopts the following process steps:
[0024] 1. First put 30% water and 7% zinc powder on 1.6m 3 In the beating barrel, mix and beat at room temperature, and then put it into the 6m 3 In the barrel reactor, 13% sulfur dioxide gas is added, and the reaction is carried out at a temperature of 30° C. to form zinc dithionite. The reaction time is 120 minutes; the pressure is normal pressure.
[0025] 2. Put zinc dithionite into 10m 3 Add 14% formaldehyde and 5% zinc powder into the two-three reaction pot, and react at 95°C to form basic zinc formaldehyde sulfoxylate, reaction time: 75 minutes; pressure: normal pressure.
[0026] 3. Put 10m 3 The basic zinc hydrogen sulfoxylate formaldehyde in the two or three reaction pots is precipitated, the supernatant is removed, and 22% so...
Embodiment 2
[0034] The component ratio of the low-zinc carved white block of the present invention is by weight percentage:
[0035] The production method of the low-zinc carved white block of the present invention adopts the following process steps:
[0036] 1. Put 32% water and 6.5% zinc powder on 1.6m 3 In the beating barrel, mix and beat at room temperature, and then put it into the 6m 3 In the barrel reactor, 12.5% sulfur dioxide gas is added, and the reaction is carried out at a temperature of 40° C. to form zinc dithionite. The reaction time is 110 minutes; the pressure is normal pressure.
[0037] 2. Put zinc dithionite into 10m 3 Add 15% formaldehyde and 5.5% zinc powder into the two-three reaction pot, and react at 100°C to form basic zinc formaldehyde sulfoxylate, reaction time: 68 minutes; pressure: normal pressure.
[0038] 3. Put 10m 3 The basic zinc hydrogen sulfoxylate formaldehyde in the two or three reaction pots is precipitated, the supernatant is removed, and 21%...
Embodiment 3
[0046] The component ratio of the low-zinc carved white block of the present invention is by weight percentage:
[0047] The production method of the low-zinc carved white block of the present invention adopts the following process steps:
[0048] 1. First put 34% water and 6% zinc powder on 1.6m 3 In the beating barrel, mix and beat at room temperature, and then put it into the 6m 3 In the barrel reactor, add 12% sulfur dioxide gas, and react to zinc dithionite at a temperature of 50° C., reaction time: 100 minutes; pressure: normal pressure.
[0049] 2. Put zinc dithionite into 10m 3Add 16% formaldehyde and 5% zinc powder into the two-three reaction pot, and react at 105°C to form basic zinc formaldehyde sulfoxylate, reaction time: 60 minutes; pressure: normal pressure.
[0050] 3. Put 10m 3 The basic zinc hydrogen sulfoxylate formaldehyde in the two or three reaction pots is precipitated, the supernatant is removed, and 20% sodium hydroxide is added to react again, and ...
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