Modified water-based resin composition
A technology of water-based resin and composition, which is applied in the field of polyurethane resin composition and modified water-based resin composition, can solve the problem of not fully improving the dispersibility and usable time of water-based polyurethane resin composition at the same time, not yet obtaining usable time, Reduce the appearance of the coating, etc., to achieve the effect of excellent coating appearance, prolonging the service life and reducing viscosity
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[0089] The following discloses examples and compares comparative examples to describe the present invention in more detail, so as to clarify the constitution of the present invention and verify the rationality of each requirement of the constitution of the present invention.
Synthetic example
[0091] 161.7 g of polyol A (polytetramethylene glycol: Mn=2000f=2), 2,2-dihydroxy 10.5 g of methacrylic acid (DMPA) and 63.8 g of dipropylene glycol dimethyl ether (DMDPG) were dissolved by heating at 90° C. for 10 minutes. After cooling to 60°C, 102.9 g of isocyanate A (isopropanol-modified allophanate compound of HDI: NCO=19.1%) was charged, and reacted at 80°C for 2 hours to obtain a carboxyl-containing isocyanate group-terminated preform. polymer solution. The isocyanate content of this prepolymer solution was 3.40%, and the amount of carboxylic acid introduced into the prepolymer was 0.75 mmol / g.
[0092] Then, after adding 7.9 g of triethylamine (TEA) to neutralize the carboxyl group, add 497.8 g of water and 5.4 g of diethyltriamine (DETA) while stirring, and carry out emulsification and water and amine at 30°C for 12 hours. induced chain reaction. When it was confirmed by FT-IR that there was no isocyanate group, filling was performed to obtain an aqueous polyuretha...
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Abstract
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