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Fluorescent quick detection device for benzopyrene (a) in food

A detection device, a benzo-based technology, is applied in fluorescence/phosphorescence, preparation of test samples, color/spectral property measurement, etc., and can solve the problems affecting the accuracy of detection results, many processing steps, interference separation and quantitative detection, etc. To achieve the effect of simplifying the sample pretreatment process, suppressing spectral interference, and accurate quantification

Active Publication Date: 2008-04-30
XIAMEN UNIV
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

With my country's accession to WTO, import and export coastal cities will have higher and higher inspection requirements for polycyclic aromatic hydrocarbons such as benzo(a)pyrene in foodstuffs. However, due to the complexity of existing detection methods, many quality inspection The department failed to actually carry out the work
[0004] The analysis of PAHs in food mainly has the following three problems: (1) Most PAHs in food exist in trace levels, which are easy to be further lost during the extraction and purification process, which affects the accuracy of the test results; (2) some Organic compounds will be extracted together with polycyclic aromatic hydrocarbons, which will interfere with the following separation and quantitative detection; (3) Many polycyclic aromatic hydrocarbons have similar structures, and the separation and detection of these compounds is more difficult
Sample pretreatment is quite cumbersome and time-consuming, requires a large amount of labor, and cannot meet the requirements of rapid detection, and due to many processing steps, it may also lead to the loss of the analyte benzo(a)pyrene, reducing the reliability of the determination

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  • Fluorescent quick detection device for benzopyrene (a) in food
  • Fluorescent quick detection device for benzopyrene (a) in food
  • Fluorescent quick detection device for benzopyrene (a) in food

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Embodiment Construction

[0027] The following embodiments will further illustrate the present invention in conjunction with the accompanying drawings.

[0028]Referring to Figures 1-3, the present invention has an optical part I, a control and signal processing part II and a power supply part III. The optical part I is equipped with a light source 1, an excitation monochromator 2, a sample chamber 3, a sample cell 4, a cryogenic device 7, an emission monochromator 5 and a detector 6, and the mixed light emitted by the light source 1 is split by the excitation monochromator 2 , the obtained monochromatic excitation light 17 enters the sample chamber 3 and excites the sample in the sample pool 4 located in the sample chamber 3, and the fluorescence 18 emitted by the sample in the sample pool 4 enters the detector 6 after being split by the emission monochromator 5 , the cryogenic device 7 is connected to the sample chamber 3 via an optical fiber 8 . The cryogenic device 7 is composed of a Dewar bottle ...

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Abstract

The invention discloses a fluorescence rapid detection device for benzo(a)pyrene in food, and relates to a fluorescence detection device. A rapid fluorescence detection device for benzo(a)pyrene in food with simple method, low equipment cost and fast measurement is provided. It is equipped with optical part, control and signal processing part and power supply part. The optical part is equipped with light source, excitation monochromator, sample chamber, sample pool, cryogenic device, emission monochromator and detector. The control and signal processing part is equipped with a controller, a signal amplification and differentiation module, an A / D conversion card and a computer. The power supply part is provided with a light source power supply and a detector power supply.

Description

technical field [0001] The invention relates to a fluorescence detection device, in particular to a rapid fluorescence detection device for benzo(a)pyrene in food. Background technique [0002] Polyaromatic hydrocarbons (PAHs) are a class of compounds in which at least two benzene rings are connected in the form of fused rings. crops and food. Benzo(a)pyrene has become a representative substance of polycyclic aromatic hydrocarbons due to its wide distribution, stable properties and strong carcinogenicity. The way that benzo(a)pyrene harms humans is mainly food pollution, especially the content of benzo(a)pyrene in processed food (such as smoked food, baked food and fried food, etc.) is relatively high, so it is necessary to strictly monitor. [0003] The contamination of food by benzo(a)pyrene has attracted extensive attention from all over the world, and many countries have stipulated corresponding dietary intake and food limit standards. my country's allowable limit st...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/64G01N1/28G01N21/31
Inventor 李耀群邹哲祥林国春周娜李呐张伟
Owner XIAMEN UNIV
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