Use of modified polysaccharide rich in galactose in preparing medicine for preventing the colitis cancer
A technology of galactose and colitis, applied in the field of application of galactose-rich modified polysaccharides in the preparation of drugs to prevent colitis from becoming cancerous, and can solve problems that have not yet been retrieved
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[0025] The preparation method of the above-mentioned modified polysaccharide rich in galactose is as follows:
[0026] The preparation method of the modified natural gum is to hydrolyze the natural gum containing galactose through polysaccharase (pH=4-5), or through alkali (pH=9-10) and acid (pH=3-5) After hydrolysis, or methanol saponification (1N NaOH, 24 hours), or sodium borohydride reduction, alcohol precipitation, dialysis, concentration, and freeze-drying, the modified natural gum was obtained. The modified natural gum is hydrolyzed by galactosidase (pH=4-6, 37° C.), alcohol precipitation, dialysis, concentration and freeze-drying. Gel chromatography or molecular weight cut-off obtains the modified natural gum containing galactose with target molecular weight (5000-50000Da). Its specific preparation method is described in detail through Examples 1-4.
[0027] The extraction method of the modified plant polysaccharide is as follows: crushing aloe vera, medlar, apple, j...
Embodiment 1
[0032] Take 100g of pectin, after slightly moistening, incubate with pectinase at 37°C for 4 hours (pH=4-6), adjust the pH value to neutral, overnight, use HPLC to detect the degree of esterification, alcohol precipitation, dialysis, and molecular weight determination. Gel chromatography or molecular weight cut-off to obtain pectin with a molecular weight of 5000-50000Da.
Embodiment 2
[0034] Take 100g of guar gum, after slightly moistening, reflux for 4 hours (pH = 9-10), adjust the pH value to neutral, overnight, and then reflux for 2 hours (pH = 3-4), alcohol precipitation, dialysis, concentration, freezing Dry. It was hydrolyzed by galactosidase (pH=4-6, 37°C), alcohol precipitation, dialysis, concentration and lyophilization. Gel chromatography or molecular weight cut-off obtains the guar gum of target molecular weight (5000-50000Da).
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