Complex printing gum for reactive dye and preparation method thereof

A technology for printing paste and reactive dyes, applied in the field of paste, can solve the problems of poor electrolyte resistance, hard fabric printing feel, and hard feel, and achieve the effect of enhancing water holding capacity

Active Publication Date: 2008-12-03
HUBEI DAYA BIOLOGICAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The applicant has carried out a large number of application tests on various natural polymer pastes and synthetic pastes, and found that most of them are prone to cause reactive dyes and The printing paste undergoes cross-linking reac...

Method used

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  • Complex printing gum for reactive dye and preparation method thereof
  • Complex printing gum for reactive dye and preparation method thereof
  • Complex printing gum for reactive dye and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0103] Preparation of component A:

[0104] Take 3000 kg of 10% wood pulp and put it into a 5000L reaction kettle, add 50.5L of 33% industrial hydrogen chloride (density: 1.08g / ml), heat up to 90°C, acidify for 12 hours under constant stirring, cool down and use Rinse in cold water until neutral and tumble dry until ready to use. Take 200 kg of wood pulp powder treated as above, put it into a 1000L reaction kettle, add 800L of 95% isopropanol as a solvent, raise the temperature to 70°C, add 26.6 kg of sodium hydroxide for alkalization reaction for 2 hours, and then add chlorine 116 kg of acetic acid, carried out etherification reaction under the condition of keeping the temperature constant for 2 hours, cooled to 40° C., adjusted the pH value to 10, added 14 kg of sodium hypochlorite for carboxylation reaction for 90 minutes, and centrifuged to obtain component A.

[0105] Preparation of component B:

[0106] Put 200 kg of potato starch in a 1000L reaction kettle, add 700L o...

Embodiment 2

[0110] Preparation of component A:

[0111] Put 4000 kg of 10% wood pulp into a 5000L kneader, add 70L of 33% industrial hydrogen chloride, heat up to 90°C, acidify for 12 hours under continuous stirring, cool down and rinse with cold water until neutral, and dry for later use. Take 600 kg of wood pulp powder treated above, add it to a 3000L reaction kettle, add 1000L of 95% isopropanol as a solvent, heat up to 70°C, add 80 kg of sodium hydroxide, alkalinize for 2 hours, and then add chlorine 350 kg of acetic acid, heat-retaining etherification reaction for 2 hours, lowered to 40 ° C, adjusted the pH value to 10, added 40 kg of sodium hypochlorite, carboxylated for 90 minutes, and centrifuged to obtain component A.

[0112] Preparation of component B:

[0113] Add 600 kg of potato starch into a 3000L kneader, add 1200L of 95% isopropanol, heat up to 35°C, add 400 kg of sodium hydroxide to alkalize the solution, add 3 kg of epichlorohydrin for 1.5 hours of crosslinking reactio...

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Abstract

The invention relates to a paste applied during the printing process of active dyes of textiles and the preparation method thereof. The method comprises the steps as follows: subjecting wood pulp to acidification treatment, alkalization treatment, etherealization treatment and carboxylation treatment to obtain a component (A); subjecting potato starch to alkalization, cross-linking and grafting treatment, introducing sulfoethyl group, conducting etherealization treatment to obtain a component (B); taking kollidon as a component (C); and mixing the components (A), (B) and (C) at a ratio of 5:4:1. The paste as a novel printing paste can improve the printing performance, reduce the production cost and replace sodium alginate.

Description

technical field [0001] The invention relates to a paste used in the printing process of textile reactive dyes. Background technique [0002] The process of textile reactive dye printing requires the use of paste as a carrier to transfer reactive dyes and auxiliaries to textile fibers. Since the advent of reactive dyes for more than 50 years, sodium alginate has been used in the printing and dyeing industry as a commonly used paste for reactive dye printing. Sodium alginate has the excellent properties of brightly printed textile patterns, clear line outlines, good plasticity and permeability, but a large amount of -COO- in sodium alginate molecules has a strong hydration effect, resulting in higher Newtonian viscosity and fluidity. Transgender is not ideal. [0003] In recent years, due to the discovery of the physiological activity of sodium alginate and its application in the food industry, its price has continued to rise, which has greatly increased the production cost ...

Claims

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Application Information

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IPC IPC(8): D06P1/44D06P1/38
Inventor 陈学俊张恒凤雷江平郑琼
Owner HUBEI DAYA BIOLOGICAL TECH CO LTD
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