Modification technique of synthetic resin impregnated timber
A technology for impregnating wood and synthetic resin, which is applied in the direction of impregnating wood, wood processing appliances, wood treatment, etc. Increased, stable product quality, and improved production efficiency
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Embodiment 1
[0015] 1 Preparation of impregnation solution: add 14kg (149 moles) of phenol into the reaction kettle, raise the temperature to 42°C, add 2.4kg (14.9 moles) of 25% liquid caustic soda under stirring, heat up to 65°C within 55min after adding, At 78°C, add 25.4 kg (312.9 moles) of 37% formaldehyde successively within 80 minutes, keep at 80-85°C for 3 hours after adding, cool down to below 25°C and discharge.
[0016] Quality index: The appearance of 10% phenolic resin solution is a brown-red transparent liquid, the wavelength is 496nm, the thickness of the cuvette is 10mm, and its optical density is 1.298.
[0017] 2 impregnation: the density of 399 (kg / m 3 ) quality 6.4kg poplar plank (200×20×4cm) into the autoclave, airtight, connect to the vacuum system, vacuumize at 0.05MPa for 20min, then pump 20.0kg of the impregnating liquid working solution with a mass fraction of 12%, Change the vacuum system to a pressurized system, pressurize at 0.7MPa for 1 hour, and take out the ...
Embodiment 2
[0022] 1 Preparation of impregnating solution: add 14kg (149 moles) of phenol to the reaction kettle, raise the temperature to 43°C, add 2.6kg (16.4 moles) of 25% liquid caustic soda under stirring, and raise the temperature to 70°C within 70 minutes after adding. At 74°C, add 27.8 kg (342.7 moles) of 37% formaldehyde successively within 60 minutes, keep at 80-85°C for 3 hours after adding, cool down to below 25°C and discharge.
[0023] Quality index: The appearance of 10% phenolic resin solution is a brown-red transparent liquid, the wavelength is 496nm, the thickness of the cuvette is 10mm, and its optical density is 1.280.
[0024] 2 impregnation: the density 430 (kg / m 3 ) quality 6.9kg poplar plank (200×20×4cm) into the autoclave, airtight, connect to the vacuum system, vacuumize at 0.085MPa for 25min, then pump 21.0kg of the impregnating liquid working solution with a mass fraction of 15%, Change the vacuum system to a pressurized system, pressurize at 0.8MPa for 55 min...
Embodiment 3
[0029] 1 Preparation of impregnation solution: add 14kg (149 moles) of phenol to the reaction kettle, raise the temperature to 44°C, add 2.9kg (17.9 moles) of 25% liquid caustic soda under stirring, heat up to 70°C within 50min after adding, and heat up to 70°C within 50min. At 78°C, add 30.2 kg (372.5 moles) of 37% formaldehyde successively within 70 minutes, keep at 72-85°C for 3 hours after adding, cool down to below 25°C and discharge.
[0030] Quality index: The appearance of 10% phenolic resin solution is a brown-red transparent liquid, the wavelength is 496nm, the thickness of the cuvette is 10mm, and its optical density is 1.310.
[0031] 2 impregnation: the density 455 (kg / m 3 ) quality 7.3kg poplar wood plank (200×20×4cm) into the autoclave, airtight, connect to the vacuum system, vacuumize at 0.065MPa for 30min, then pump 22.5kg of the impregnating liquid working solution with a mass fraction of 10%, Change the vacuum system to a pressurized system, pressurize at 0...
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