Water-scraped without set-off intaglio ink
A technology of gravure printing ink and smearing, applied in ink, printing, printing devices, etc., can solve the problems of poor metal texture of printed products, affecting the aesthetic effect, and discounting the anti-counterfeiting strength
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Embodiment A1
[0055] 10.1 parts of tower oil fatty acid, 6.8 parts of linoleic acid, 7.8 parts of glycerin, 3.4 parts of pentaerythritol, 5.7 parts of phthalic anhydride and an appropriate amount of xylene are heated up to 200 ° C under the protection of nitrogen, and the temperature is kept Esterification, measuring the acid value of the system during the reaction, and cooling down when the acid value reaches 4, to obtain an ortho-phenyl alkyd resin with an oil degree of 55%. Take a total of 32 parts of the above resin, add 45 parts of dodecane solvent, 10 parts of dipropylene glycol dimethyl ether solvent and heat up to about 80°C, add 7 parts of toluene diisocyanate (TDI) dropwise and keep it warm for 2 hours until the viscoelastic ratio is 4. Add 0.05 parts of dibutyltin dilaurate and 0.5 parts of methanol, keep warm for 1 hour, use about 4-5 parts of solvent to adjust the product to a viscosity of 12Pa.S / 40℃, and a viscoelastic ratio of 6. That is, the vehicle component A1 is obtained....
Embodiment A2-A11
[0057] The preparation method is the same as in Example 1, and the reaction materials and dosage ratios are shown in Table 1.
[0058] Table 1
[0059] serial number
[0060] Dibutyltin dilaurate
[0061] Cobalt naphthenate
[0062] Preparation of vehicle component B
Embodiment B1
[0064]Add 30 parts of tung oil, 25 parts of flax oil, 10 parts of glycerin, and 4 parts of pentaerythritol into the reaction kettle. When the temperature reaches 160°C, add 0.05 parts of catalyst lithium hydroxide, and the transesterification reaction occurs at 240°C under the protection of nitrogen. After the alcoholysis is qualified (reaction product: 95% ethanol = 1:5, the solution is clear and transparent), add 25 parts of isophthalic acid, 0.02 parts of catalyst zinc oxide and an appropriate amount of methyl isobutyl ketone as a medium solvent, and keep warm at 230 ° C. Stop the reaction when the acid value reaches 15, and adjust the viscosity to 6.2 Pa.S / 40°C with dodecane solvent (about 6 parts) to obtain m-benzene alkyd resin B1 with an oil degree of 62%.
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