Reinforced textile type glass fiber treating compound and preparation thereof

A sizing and textile-type technology, which is applied in the field of reinforced textile glass fiber sizing and its preparation, can solve the problems of material waste and complicated process, and achieve the effect of no washing process, simple preparation and use process, and good clustering

Inactive Publication Date: 2009-05-27
上海世鹏聚氨酯科技发展有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] The traditional textile glass fiber sizing is mainly made of starch and paraffin. Before the compounding of glass fiber reinforced plastic products, this type of sizing needs to heat wa

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0046] Example 1

[0047] Preparation method of reinforced textile glass fiber sizing agent:

[0048] A. Hydrolysis of silane coupling agent:

[0049] Add acetic acid to 500 grams of deionized water to adjust the pH to 3 to 4, stir slowly at 300 rpm, add 3 grams of silane coupling agent, and continue to stir for 30 to 50 minutes. When the solution is clear and there are no oil drops, the stirring can be stopped. And control the PH value to be less than 6, and make the coupling agent hydrolysate;

[0050] B. The dissolution preparation of solid antistatic agent:

[0051] After heating 100 grams of deionized water to 80°C, add 1 gram of solid antistatic agent and stir slowly until all is dissolved, then cool to room temperature to prepare an antistatic agent solution;

[0052] C. Add the above coupling agent hydrolyzate and antistatic agent solution into the preparation kettle, add 0.5 g of lubricant, 80 g of polyvinyl acetate emulsion, 20 g of polyester emulsion, 50 g of epoxy resi...

Example Embodiment

[0053] Example 2

[0054] A. Hydrolysis of silane coupling agent:

[0055] Add acetic acid to 500 grams of deionized water to adjust the pH to 3~4, slowly stir at 300 rpm, add 4 grams of silane coupling agent, and continue to stir for 30-50 minutes. When the solution is clear and there is no oil drop phenomenon, the stirring can be stopped. , And control the pH value to be less than 6, to make the coupling agent hydrolysate;

[0056] B. The dissolution preparation of solid antistatic agent:

[0057] After heating 100 grams of deionized water to 80°C, add 2 grams of solid antistatic agent, stir slowly, and then cool to room temperature after all is dissolved;

[0058]C. Add the above-prepared coupling agent hydrolysate and antistatic agent solution into the configuration kettle, add 0.4 g of lubricant, 60 g of polyvinyl acetate emulsion, 40 g of polyester emulsion, and 40 g of epoxy resin emulsion. , Polyurethane emulsion 6 grams, surfactant 4 grams and the remaining part of deioni...

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PUM

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Abstract

The invention provides an impregnating compound for reinforced textile glass fibers, which takes novel organic polymer materials as a main body. The impregnating compound comprises the following compositions by weight percentage: 5 to 10 percent of polyvinyl acetate emulsion, 1 to 4 percent of polyester emulsion, 2 to 8 percent of epoxy resin, 0.2 to 2 percent of polyurethane emulsion, 0.01 to 0.2 percent of lubricant, 0.1 to 0.5 percent of coupling agent, 0.05 to 0.3 percent of antistatic agent, 0.2 to 3 percent of surfactant, 0.05 to 1 percent of acetic acid, and the balance being deionized water. The impregnating compound has good convergence, lubricity, film-forming property and antistatic property; the glass fibers which are treated by the impregnating compound have the characteristics of bending resistance, flexibility, tensile resistance, good solubility with resin and so on; and the impregnating compound is suitable for treating the surfaces of various reinforced textile glass fibers.

Description

technical field [0001] The present invention relates to reinforced textile glass fiber sizing agent and preparation method thereof, with novel organic macromolecule film-forming agent, including polyvinyl acetate emulsion, polyester emulsion, epoxy resin and polyurethane emulsion, coupling agent, lubricant as The main body has the advantages of flexibility, lubrication, bending resistance and tensile resistance, and is suitable for surface treatment of various textile fibers. Background technique [0002] The traditional textile glass fiber sizing is mainly made of starch and paraffin. Before the compounding of glass fiber reinforced plastic products, this type of sizing needs to heat wash the glass fiber. The use of heating and cleaning to remove the sizing agent leads to complex processes, waste of materials, and unfavorable factors such as the need to dispose of washing waste. In order to overcome the shortcomings of the traditional technology, it is necessary to develop...

Claims

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Application Information

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IPC IPC(8): C03C25/26
Inventor 孙寿鹏孙寿松孙寿彬
Owner 上海世鹏聚氨酯科技发展有限公司
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