Titanium-aluminum intermetallic compound-carbon nano tube compound material preparation method and products
A technology of intermetallic compounds and carbon nanotubes, applied in the preparation of titanium-aluminum matrix composite materials, the preparation method of titanium-aluminum intermetallic compound-carbon nanotube composite materials and its products, to achieve the effect of improving comprehensive performance
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Embodiment 1
[0025] (1) Put Ti and Al with a purity of 99.5% into Ti 48 Al 52 The required atomic ratio is arc-melted in an argon atmosphere to make it evenly mixed and cooled to obtain Ti 48 Al 52 master alloy ingot;
[0026] (2) The master alloy ingot is ground into a powder with an average grain size less than 300 μm by mechanical grinding, and dried with a dryer;
[0027] (3) Mix carbon nanotubes and titanium-aluminum alloy powder with a volume percentage of 1%, and grind the mixed powder composed of carbon nanotubes and titanium-aluminum alloy powder with a low-power mechanical alloying equipment, and the grinding time is 15 Hour. After the mixed powder is evenly mixed, put it into the dryer and dry it for a long time at a temperature of 473K to remove the moisture contained in the mixed powder;
[0028] (4) Compacting the composite powder obtained in step (3) in a mold with a diameter of 42 mm, the pressing pressure is 150 MPa, and the pressing time is 30 minutes;
[0029] (5) ...
Embodiment 2
[0033] (1) Ti and Al with a purity of 99.7% are pressed by Ti 50 Al 50 The required atomic ratio is arc-melted in an argon atmosphere to make it evenly mixed and cooled to obtain Ti 50 Al 50 master alloy ingot;
[0034] (2) The master alloy ingot is ground into a powder with an average grain size less than 300 μm by mechanical grinding, and dried with a dryer;
[0035] (3) Mix carbon nanotubes and titanium-aluminum alloy powder with a volume percentage of 2%, and grind the mixed powder composed of carbon nanotubes and titanium-aluminum alloy powder with a low-power mechanical alloying device, and the grinding time is 18 Hour. After the mixed powder is evenly mixed, put it into the dryer and dry it for a long time at a temperature of 473K to remove the moisture contained in the mixed powder;
[0036] (4) Compacting the composite powder obtained in step (3) in a mold with a diameter of 42 mm, the pressing pressure is 165 MPa, and the pressing time is 45 minutes;
[0037] (...
Embodiment 3
[0041] (1) Ti and Al with a purity of 99.8% are pressed by Ti 30.5 Al 69.5 The required atomic ratio is arc-melted in an argon atmosphere to make it evenly mixed and cooled to obtain Ti 30.5 Al 69.5 master alloy ingot;
[0042] (2) The master alloy ingot is ground into a powder with an average grain size less than 300 μm by mechanical grinding, and dried with a dryer;
[0043] (3) Mix carbon nanotubes and titanium-aluminum alloy powder with a volume percentage of 5%, and use low-power mechanical alloying equipment to grind the mixed powder composed of carbon nanotubes and titanium-aluminum alloy powder, and the grinding time is 24 Hour. After the mixed powder is evenly mixed, put it into the dryer and dry it for a long time at a temperature of 473K to remove the moisture contained in the mixed powder;
[0044](4) Compacting the composite powder obtained in step (3) in a mold with a diameter of 42 mm, the pressing pressure is 180 MPa, and the pressing time is 60 minutes; ...
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Abstract
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