Phenyl-imidazopyridine type trivalent-iridium organometallic complex and organic electro-phosphorescent luminescent device thereof
An azolopyridine and organometallic technology, which is applied in the field of organic phosphor photoluminescent devices, can solve the problems of insufficient photoelectric properties such as color coordinates, brightness, and efficiency, and achieve excellent color coordinates, advanced and flexible technology, and simple and flexible manufacturing process Effect
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example 1
[0039] Example 1: Synthesis of Ligand BrPIPy:
[0040] In a 250ml three-necked flask equipped with stirring, a thermometer, a gas introduction device, and a reflux condenser, nitrogen gas was introduced for 15 minutes, and 2,4'-dibromoacetophenone 32.6g (0.117mol), 2-aminopyridine 10.4 g (0.111mol), NaHCO 3 l3 (0.155mol) g, 62 g of absolute ethanol, after stirring for 30 min, heat up and reflux for 2 to 3 h. After cooling down to room temperature, the reaction solution was poured into 10 times the volume of water to precipitate a solid, filtered, and washed with water until neutral. The filter cake was boiled and washed with ethanol for 1 h, cooled to room temperature, filtered, and dried to obtain a light brown crude product of 2-(4'-bromo)phenylimidazopyridine (BrPIPy). The crude product was recrystallized from 27 times ethanol to obtain 22.3 g of white crystalline product BrPIPy, HPLC≥99%.
example 2
[0041] Example 2: Synthesis of Ligand PIPy:
example 1
[0042] Referring to the synthesis and purification method of Example 1, 21.1 g (0.106 mol) of 2-bromoacetophenone was reacted with 9.4 g (0.1 mol) of 2-aminopyridine to obtain 15.9 g of the white product 2-phenylimidazopyridine (PIPy). HPLC≥99%.
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