Separator
A technology of heat-resistant layer and laminated porous film, which is applied in the direction of electrical components, structural parts, battery pack parts, etc., can solve the problem of unsatisfactory capacity of non-aqueous electrolyte secondary batteries, and achieve excellent high-current discharge characteristics, durability high heat effect
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[0111] (1) Manufacture of coating liquid
[0112] After dissolving 272.7 g of calcium chloride in 4200 g of NMP, 132.9 g of p-phenylenediamine was added and completely dissolved. To the obtained solution, 243.3 g of terephthaloyl chloride (hereinafter, abbreviated as TPC) was slowly added for polymerization to obtain a para-aramide, which was further diluted with NMP to obtain a para-aramide solution (A) with a concentration of 2.0% by weight. To 100 g of the obtained para-aramid solution, 4 g of alumina powder (Sumiko Random, AA03 manufactured by Sumitomo Chemical Co., Ltd., AA03, number average particle diameter: 0.3 μm) containing nearly spherical particles was added as a filler, mixed, and treated with a nanomachine three times. , and further filtered through a 1000-mesh metal mesh, degassing was performed under reduced pressure to obtain a slurry coating solution (B). The weight of alumina powder (filler) was 67% by weight relative to the total weight of para-aramid and ...
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