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Production process for pressuring and condensing trichlorosilane synthesized product

A technology for synthesizing products, trichlorosilane, applied in the direction of silicon halide compounds, halosilanes, etc., can solve the problems of extended maintenance period, low condensation efficiency of synthetic products, and large refrigerant consumption, so as to improve condensation efficiency and reduce Refrigerant consumption and the effect of extending the service life

Inactive Publication Date: 2010-01-20
CHINA SILICON CORP LTD
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Problems solved by technology

[0007] In order to solve the above problems, the present invention provides a production process for pressurized condensation of trichlorosilane synthesis products. This production process effectively solves the problems of low condensation efficiency of synthesis products and high refrigerant consumption, and prolongs the life of the entire system. Maintenance cycle

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  • Production process for pressuring and condensing trichlorosilane synthesized product

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Embodiment Construction

[0024] Explanation again: the trichlorosilane synthesis product described in the present invention refers to the mixed gas after the synthesis of industrial silicon powder and HCl, and the mixed gas contains H in addition to the dust. 2 , HCl, SiHCl 3 、SiH 2 Cl 2 or SiCl 4 Wait. The trichlorosilane synthesis product referred to herein may also refer to the mixed gas.

[0025] to combine figure 1 , the production process of the pressurized condensation of the trichlorosilane synthesis product of the present invention is a water cooler before compression, a deep cooler before compression, a hydrogen compressor, a deep cooler after compression, a synthetic product storage tank and a dry tail gas recovery system Implementation, the production process includes five processes of water cooling before compression, cryogenic cooling before compression, pressurization by hydrogen compressor, cryogenic cooling after compression and dry recovery of exhaust gas. The five processes are...

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Abstract

The invention discloses a production process for pressuring and condensing trichlorosilane synthesized products, which is implemented in a before-compression water cooler, a before-compression copious cooler, a hydrogen compressor, an after-compression copious cooler, a synthetic product storage tank and a tail gas dry-method recovery system. The production process comprises five processes of before-compression water cooling, before-compression copious cooling, hydrogen compressor pressuring, after-compression copious cooling and tail gas dry-method recovery. The invention effectively improves the condensation efficiency of the trichlorosilane synthesized product; after one-time pressuring and condensation, the recovery of chlorosilane is more than 90%; and then after being processed by the tail gas dry-method recovery system, the product is pressured and condensated once again, the condensation recovery of chlorosilane is more than 99%. The production process can reduce refrigerant consumption and extend the service cycle of hydrogen compressors.

Description

technical field [0001] The invention belongs to the technical field of chemical production, and in particular relates to a production process of pressurized condensation of a trichlorosilane synthesis product. Background technique [0002] Trichlorosilane is an important intermediate for the manufacture of silane coupling agents and other organosilicon products, and is also an important raw material for the preparation of semiconductor-grade polysilicon and solar-grade polysilicon. With the increasing international and domestic demand for polysilicon, the stable supply of high-quality and large-volume trichlorosilane is particularly important. [0003] The synthesis of trichlorosilane mostly adopts atmospheric pressure synthesis process, the production capacity of a single equipment and the utilization rate of raw materials are low, and the system configuration is not perfect, such as no special liquid chlorine vaporization system, no liquid chlorine or hydrogen chloride deh...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01B33/107
Inventor 严大洲肖荣晖毋克力杜俊平
Owner CHINA SILICON CORP LTD
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