Microwave reaction synthesis method for endogenous metal matrix composite material
A composite material and microwave reaction technology, applied in the field of microwave reaction synthesis method, to achieve the effect of purifying the matrix, shortening the preparation cycle, and refining the structure
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[0027] Example 1: Al-TiO 2 -B reaction system
[0028] (1) Prepare the reaction sample with Al, TiO 2 , B powder according to the set reinforcement (TiB 2 And Al 2 O 3 ) Volume fraction (such as 30%), from the chemical reaction formula: 4Al+3TiO 2 +6B→3TiB 2 +2Al 2 O 3 By stoichiometric calculation, the reaction formula Meet the thermodynamic conditions of the reaction. It is calculated that 20g reaction sample requires 15.43g Al powder and TiO 2 Powder 4.57g and B powder 0.57g. Then put it in a ball mill tank, mix it with a ball mill at a ball-to-powder ratio of 5:1 and a rotation speed of 300p.r.m, and then extrude it at a pressure of 120MPa to form a compact sample;
[0029] (2) Sample loading Put the compact sample into the reaction device, see figure 1 ; Pay attention to the following points when loading samples: 1) Bare the top of the compact sample to ensure the accuracy of infrared temperature measurement on the top of the sample; 2) Do not block the side monitoring hole w...
Example Embodiment
[0035] Example 2: Al-ZrO 2 system
[0036] (1) Prepare the reaction sample by Al, ZrO 2 Powder according to the set reinforcement (Al 3 Zr and Al 2 O 3 ) Volume fraction (such as 30%), from the chemical reaction formula: 13Al+3ZrO 2 →3Al 3 Zr+2Al 2 O 3 By stoichiometric calculation, the reaction formula Meet the thermodynamic conditions of the reaction. By calculation, a 20g reaction sample requires 16.1g Al powder and ZrO 2 3.9g powder, then put it into a ball mill tank, mix it with a ball mill at a ball-to-powder ratio of 5:1 and a rotation speed of 300p.r.m, and then extrude it at a pressure of 120MPa to form a compact sample;
[0037] (2) Sample loading Put the compact sample into the reaction device, see figure 1 ; Pay attention to the following points when loading samples: 1) Bare the top of the compact sample to ensure the accuracy of infrared temperature measurement on the top of the sample; 2) Do not block the side monitoring hole with SiC absorber to ensure the side durin...
Example Embodiment
[0043] Example 3: Al-Ni 2 O 3 reaction system
[0044] (1) Prepare the reaction sample by combining Al and Ni 2 O 3 Powder according to the set reinforcement (Ni 2 Al 3 And Al 2 O 3 ) Volume fraction (such as 20%), from the chemical reaction formula: 5Al+Ni 2 O 3 →Ni 2 Al 3 +Al 2 O 3 By stoichiometric calculation, the reaction formula Meet the thermodynamic conditions of the reaction. It is calculated that 20g reaction sample requires 13.26g Al powder and Ni 2 O 3 1.74g powder, then put it into a ball mill tank, mix it with a ball mill at a ball-to-powder ratio of 5:1 and a rotation speed of 300p.r.m, and then extrude into a billet at a pressure of 120MPa to make a compact sample;
[0045] (2) Sample loading Place the compact sample into the reaction device (see figure 1 ); Pay attention to the following points when loading the sample: 1) Bare the top of the compact sample to ensure the accuracy of infrared temperature measurement on the top of the sample; 2) Do not block the side ...
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