Semi-electroactive material containing organic compounds with positive or negative redox activity, method and kit for making such material, electrically controlled device and glazing using such semi-e
A technology of electroactive materials and electronic control equipment, applied in the direction of chemical instruments and methods, color-changing fluorescent materials, glass/slag layered products, etc., can solve any problems that do not describe the combination of components that complement coloring
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Embodiment 1
[0107] Embodiment 1: the preparation of electrochromic device
[0108] -with SnO 2 : F layer, glass coated with PEDOT / PSS layer;
[0109] - semi-electroactive system: ferrocene + lithium perchlorate + propylene carbonate; and
[0110] -with SnO 2 :F layer of glass.
[0111] Electrochromic devices were fabricated using bare K-glass flakes and K-glass flakes deposited with PEDOT / PSS layers (360 micron wet deposition). Before assembly, the PEDOT / PSS layer was reduced in a 1 M solution of acetonitrile and lithium perchlorate.
[0112] The PVDF self-supporting film is prepared by mixing 3.5g PVDF ( 2501), 6.5g of dibutyl phthalate and 12g of acetone. The formation was stirred for two hours before being cast on glass slides. After evaporation of the solvent, the PVDF film was removed from the glass slide under a drip of water.
[0113] A semi-electroactive solution was prepared by mixing 0.23 g of ferrocene and 0.27 g of lithium perchlorate into 40 ml of propylene carbonat...
Embodiment 2
[0116] Embodiment 2: the preparation of electrochromic device
[0117] -with SnO 2 : F layer, glass coated with PEDOT / PSS layer;
[0118] - semi-electroactive system: ferrocene + lithium trifluoromethanesulfonate + propylene carbonate; and
[0119] -with SnO 2 :F layer of glass.
[0120] Electrochromic devices were fabricated using bare K-glass flakes and PEDOT / PSS-deposited K-glass flakes (360 micron wet deposition). Prior to assembly, the PEDOT / PSS layer was reduced in a solution of acetonitrile and lithium perchlorate at a concentration of 1M.
[0121] The PVDF self-supporting film is prepared by mixing 3.5g PVDF ( 2821), 6.5g of dibutyl phthalate and 12g of acetone. The formation was stirred for two hours and cast on glass slides. After evaporating the solvent, the PVDF film was removed from the glass slide under a drip of water.
[0122] A semi-electroactive solution was prepared by mixing 0.23 g of ferrocene and 0.39 g of lithium trifluoromethanesulfonate into...
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