Downconversion frequency shift infrared radiation enhanced coating and preparation method thereof
A technology of infrared radiation and coating, applied in the field of infrared radiation coating and its preparation
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Embodiment 1
[0066] The preparation method of down-conversion frequency-shift infrared radiation enhanced coating is characterized in that it comprises the following steps:
[0067] One, the preparation of down conversion frequency shift additive: it comprises the following steps:
[0068] (1) formula composition (mass percentage): Pr 2 o 3 10%; Yb 2 o 3 10%; Er 2 o 3 10%; 3Y-ZrO 2 70%.
[0069] (2) Take 3Y-ZrO 2 The mass percentage of the formula composition is 30% and the Pr of the whole formula composition 2 o 3 , Yb 2 o 3 and Er 2 o 3 , placed in a planetary mill, and ground for 1 hour until the particle size is d 50 ≤1μm, d 90 ≤5μm, take it out and put it into a corundum crucible, put it into a high-temperature furnace, keep it warm at 1300°C for 1 hour under an oxidizing atmosphere, increase the temperature to a rate of 6°C / min, and crush it by a planetary mill after natural cooling, with a particle size of d 50 ≤1μm, d 90 ≤5μm, obtain the powder prepared in the firs...
Embodiment 2
[0110] A preparation method for down-conversion frequency-shift infrared radiation enhanced coating, which comprises the following steps:
[0111] One, the preparation method of down conversion frequency shift additive, it comprises the steps:
[0112] (1) formula composition (mass percentage): Pr2 o 3 10%; Dy 2 o 3 10%; 3Y-ZrO 2 80%.
[0113] (2) Take 3Y-ZrO 2 The mass percentage of the formula composition is 30% and the Pr of the whole formula composition 2 o 3 and Dy 2 o 3 , placed in a planetary mill, and ground for 1 hour until the particle size is d 50 ≤1μm, d 90 ≤5μm, take it out and put it into a corundum crucible, put it into a high-temperature furnace, keep it warm at 1300°C for 1 hour under an oxidizing atmosphere, and heat up at a rate of 7°C / min. After natural cooling, it is crushed by a planetary mill, and the particle size is d 50 ≤1μm, d 90 ≤5μm, obtain the powder prepared in the first step.
[0114] (3) Take 3Y-ZrO 2 70% of the formula compositio...
Embodiment 3
[0135] A preparation method for down-conversion frequency-shift infrared radiation enhanced coating, which comprises the following steps:
[0136] 1. Preparation of down-converting frequency-shifting additive: Same as Example 1.
[0137] 2. According to the mass percentage of each component: 50% of radiation synergistic enhancer, 1% of down conversion frequency shift additive, 15% of high temperature resistant base material, 32% of high temperature binder, 1% of toughening agent, paint auxiliary 1% of additives, select radiation synergistic enhancers, down conversion frequency shift additives, high temperature resistant base materials, high temperature binders, tougheners and coating additives;
[0138] Wherein, the coating additives include polyvinyl alcohol, dispersant, defoamer, film-forming agent, leveling agent and preservative, and the mass percentages of each component of the coating additives account for the down-conversion frequency-shift infrared radiation-enhanced c...
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