Method for producing oxidized starch
A production method and technology of oxidized starch, which is applied in the field of modified starch production, can solve the problems of large dosage and achieve the effects of reduced dosage, faster reaction speed and shorter reaction time
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Embodiment 1
[0013] (1). Activation: Add 1500 kg of water to 1000 kg of starch to prepare starch milk, then add 50 g of copper sulfate and stir evenly;
[0014] (2). Oxidation: add 400 kilograms of content 10% sodium hypochlorite in the starch milk after activation, control the speed of adding medicine and maintain PH=9, when PH value descends, add 4% sodium hydroxide solution, adjust PH=9 9. The temperature is controlled between 32 and 35°C, and the reaction time is 3 hours and 20 minutes;
[0015] (3). Neutralization: After the oxidation reaction is finished, add hydrochloric acid to adjust the pH of starch milk to 6.8;
[0016] (4). Drying: Centrifuge and dehydrate the starch milk, then air-dry it until the water content is ≤14%, and obtain a finished product with a carboxyl content of 1.05.
Embodiment 2
[0018] (1). Activation: Add 1500 kg of water to 1000 kg of starch to prepare starch milk, then add 100 g of copper sulfate and stir evenly;
[0019] (2). Oxidation: add 400 kilograms of content 10% sodium hypochlorite in the starch milk after activation, control the speed of adding medicine and maintain PH=9, when PH value descends, add 4% sodium hydroxide solution, adjust PH=9 9. The temperature is controlled between 32 and 35°C, and the reaction time is 2 hours;
[0020] (3). Neutralization: After the oxidation reaction is finished, add hydrochloric acid to adjust the pH of the starch milk to 6.9;
[0021] (4). Drying: Centrifuge and dehydrate the starch milk, then air-dry it until the water content is ≤14%, and obtain a finished product with a carboxyl content of 1.13.
Embodiment 3
[0023] (1). Activation: Add 1500 kg of water to 1000 kg of starch to prepare starch milk, then add 100 g of copper sulfate and stir evenly;
[0024] (2). Oxidation: Add 300 kilograms of content 10% sodium hypochlorite to the starch milk after activation, control the speed of adding medicine and maintain PH=9, when the pH value descends, add 4% sodium hydroxide solution, adjust PH=9 9. The temperature is controlled between 32 and 35°C, and the reaction time is 2 hours:
[0025] (3). Neutralization: After the oxidation reaction is finished, add hydrochloric acid to adjust the pH of the starch milk to 6.9;
[0026] (4). Drying: Centrifuge and dehydrate the starch milk, then air-dry it until the water content is ≤14%, and obtain a finished product with a carboxyl content of 0.86.
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