Nanooxide-doped green solder glass and preparation method thereof
A nano-oxide and solder glass technology, applied in the field of electronic glass, to achieve the effect of wide application, reducing softening temperature and solving poor chemical stability
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Embodiment 1
[0045] (1) The composition of the raw materials is as follows in molar percentage:
[0046] P 2 o 5 35%
[0047] ZnO 44%
[0048] B 2 o 3 10%
[0049] Al 2 o 3 3%
[0050] SiO 2 0.5%
[0051] Na 2 O 5%
[0052] MgO 0.3%
[0053] Li 2 O 0.3%
[0054] Fe 2 o 3 1%
[0055] MnO 2 0.7%
[0056] CrO 0.2%
[0057] (2) Introduction of raw materials:
[0058] Each raw material except Al 2 o 3 All are chemically pure grade raw materials, of which ZnO, SiO 2 , Fe 2 o 3 , MnO 2 are introduced as oxides, P 2 o 5 Introduced as phosphorus pentoxide, B 2 o 3 Introduced with boric acid, CrO introduced with chromium oxide, MgO, Na 2 O. Li 2 O was introduced in the form of carbonate, Al 2 o 3 Gamma nano-alumina with an average particle size of 10 nm is used for introduction.
[0059] (3) Preparation method:
[0060] ① Weigh eac...
Embodiment 2
[0072] (1) The composition of the raw materials is as follows in molar percentage:
[0073] P 2 o 5 40%
[0074] ZnO 34.5%
[0075] B 2 o 3 10%
[0076] Al 2 o 3 3%
[0077] SiO 2 1%
[0078] Na 2 O 4.5%
[0079] MgO 4%
[0080] Li 2 O 0.5%
[0081] Fe 2 o 3 0.5
[0082] MnO 2 1.5%
[0083] CrO 0.5%
[0084] (2) Introduction of raw materials:
[0085] Each raw material except Al 2 o 3 All are chemically pure grade raw materials, of which ZnO, SiO 2 , Fe 2 o 3 , MnO 2 are introduced as oxides, P 2 o 5 Introduced as phosphorus pentoxide, B 2 o 3 Introduced with boric acid, CrO introduced with chromium oxide, MgO, Na 2 O. Li 2 O was introduced in the form of carbonate, Al 2 o 3 Gamma nano-alumina with an average particle size of 10 nm is used for introduction.
[0086] (3) Preparation me...
Embodiment 3
[0096] (1) The composition of raw materials in molar percentage is
[0097] P 2 o 5 45%
[0098] ZnO 38%
[0099] B 2 o 3 5%
[0100] Al 2 o 3 1%
[0101] SiO 2 2.3%
[0102] Na 2 O 5%
[0103] MgO 1
[0104] Li 2 O 0.3
[0105] Fe 2 o 3 1.5%
[0106] MnO 2 0.2
[0107] CrO 0.7%
[0108] (2) Introduction of raw materials:
[0109] Each raw material except Al 2 o 3 All are chemically pure grade raw materials, of which ZnO, SiO 2 , Fe 2 o 3 , MnO 2 are introduced as oxides, P 2 o 5 Introduced as phosphorus pentoxide, B 2 o 3 Introduced with boric acid, CrO introduced with chromium oxide, MgO, Na 2 O. Li 2 O was introduced in the form of carbonate, Al 2 o 3 Gamma nano-alumina with an average particle size of 10 nm is used for introduction.
[0110] (3) Preparation method:
[0111] ① We...
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