Method for preparing composite water-retaining agent by adopting plant straws

A technology of plant straw and water-retaining agent, which is applied in the preparation of superabsorbent resin materials and the field of compound water-retaining agent prepared by plant straw, which can solve the problems of environmental pollution and waste of resources, and achieve simple preparation method, convenient operation and good comprehensive performance Effect

Active Publication Date: 2010-12-15
NORTHWEST NORMAL UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The main treatment method of plant straw in rural areas is burning, which

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0028] Example one

[0029] (1) Dissolve 3g of corn stover in 50mL of distilled water, heat and stir for 30min at 95℃;

[0030] (2) Adjust the temperature to 65°C, add 0.01g potassium persulfate as the initiator, and stir for 30 minutes;

[0031] (3) Add 4g of acrylamide, 1g of palygorskite clay and 0.1g of formaldehyde, and stir for 2h;

[0032] (4) Add 30mL of 1mol / L hydrochloric acid solution, heat up to 95°C, saponify for 2h; wash the product with methanol aqueous solution to pH=7;

[0033] (5) The product is placed in an oven, dried at 70°C until constant weight, ground and crushed, passed through a 40-mesh sieve, sealed and dried for storage.

[0034] Water retention agent performance: placed in tap water for 24 hours, its water absorption rate is about 900 times its own weight; placed in a 0.9% saline solution, its water absorption rate can reach 500 times its own weight; place the water retention agent saturated with water in the air, At room temperature (25℃) for 60 days, its w...

Example Embodiment

[0035] Example two

[0036] (1) Dissolve 4g of soybean straw in 60mL of distilled water, heat and stir for 15min at 60℃;

[0037] (2) Adjust the temperature to 40°C, add 0.012g potassium persulfate-ferrous sulfate as an initiator, and stir for 20 minutes;

[0038] (3) Add 12g of acrylamide, 2.6g of hydrotalcite and 0.08g of formaldehyde, and stir for 1h;

[0039] (4) Add 30mL of 1mol / L hydrochloric acid solution, heat up to 60°C, saponify for 30min; wash the product with methanol aqueous solution to pH=6;

[0040] (5) The product is placed in an oven, dried at 40°C until constant weight, ground and crushed, passed through a 40-mesh sieve, sealed and dried for storage.

[0041] Water retention agent performance: placed in tap water for 24h, its water absorption rate is about 800 times its own weight, placed in a 0.9% saline solution, its water absorption rate can reach 450 times its own weight; put the resin saturated with water in the air at room temperature The water retention rate can...

Example Embodiment

[0042] Example three

[0043] (1) Dissolve 1g of peanut shell stalks in 8mL of distilled water, heat and stir for 20min at 50℃;

[0044] (2) Adjust the temperature to 40°C, add 0.016g ammonium persulfate-sodium bisulfite as an initiator, and stir for 30 minutes;

[0045] (3) Add 10g of acrylamide, 0.6g of montmorillonite and 0.006g of N,N-methylenebisacrylamide, and stir for 2h;

[0046] (4) Add 30mL of 1mol / L hydrochloric acid solution, heat to 65°C, saponify for 1h; wash the product with methanol aqueous solution to pH=5;

[0047] (5) The product is placed in an oven, dried at 40°C until constant weight, ground and crushed, passed through a 40-mesh sieve, sealed and dried for storage.

[0048] Water retention agent performance: placed in tap water for 24h, its water absorption rate is about 850 times its own weight, placed in a 0.9% saline solution, its water absorption rate can reach 480 times its own weight; put the resin saturated with water in the air at room temperature The water...

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Abstract

The invention provides a method for preparing a composite water-retaining agent by adopting plant straws, belonging to the technical field of high-polymer materials. In the invention, the biodegradable plant straws with wide sources and low prices are used as raw materials, and graft copolymerization is carried out on the plant straws and acrylamide, clay, and the like to obtain the composite water-retaining agent with good comprehensive performance, therefore, the cost of the water-retaining agent is effectively reduced, and a new path for the application of the plant straws is sought. Meanwhile, since the composite water-retaining agent also has higher gel strength and saline alkali tolerance, the service performance of the water-retaining agent is further improved, and the service life thereof is prolonged.

Description

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Claims

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Application Information

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Owner NORTHWEST NORMAL UNIVERSITY
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