Method for performing infrared spectroscopic analysis on SBS modifier content of modified asphalt

A technology of infrared spectrum analysis and modified asphalt, applied in the field of infrared spectrum analysis of SBS modifier content in modified asphalt, can solve the problems of expensive ATR accessories, low sample signal intensity, lack of sensitivity, etc., and achieve accurate quantitative results Credible, convenient and quick to build, simple sample preparation process

Active Publication Date: 2010-12-15
ZHEJIANG COMM CONSTR GRP CO LTD +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The ATR accessory is constructed based on the principle of attenuated total reflection. The penetration depth of infrared light in the sample is shallow, only a few microns, so the signal intensity of the sample obtained is low, and it lacks sufficient sensitivity when determining the content of a small amount of modifier. large detection error
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  • Method for performing infrared spectroscopic analysis on SBS modifier content of modified asphalt
  • Method for performing infrared spectroscopic analysis on SBS modifier content of modified asphalt
  • Method for performing infrared spectroscopic analysis on SBS modifier content of modified asphalt

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Embodiment Construction

[0035] Below in conjunction with accompanying drawing and embodiment the present invention is further described.

[0036] An infrared spectroscopic analysis method for the content of SBS modifier in modified asphalt:

[0037] 1. Test equipment

[0038] Nicolet Fourier Transform Infrared Spectrometer

[0039] 2. Establishment of SBS Modified Asphalt Standard Sample and SBS Modifier Content Standard Criterion

[0040] 1) Take 0.5g of the SBS modified asphalt standard sample and dissolve it in an organic solvent; evenly coat the solution having the SBS modified asphalt standard sample on the surface of the potassium bromide salt sheet; put the potassium bromide salt sheet at 80 degrees Dry for 20 minutes;

[0041] 2) The prepared SBS modified asphalt standard sample is tested by infrared spectrum, and the measured 4000-400cm -1 Infrared transmission spectrum;

[0042] 3) Calculate 966cm on the transmission spectrum -1 and 1377cm -1 The relative ratio of the absorption peak a...

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Abstract

The invention discloses a method for performing infrared spectroscopic analysis on the SBS modifier content of modified asphalt, which comprises the following steps of: acquiring transmittance spectrum of an SBS modified asphalt sample with the known SBS modifier content by using a Fourier infrared spectrometer; computing a relative ratio A of a peak area which only belongs to a characteristic infrared absorption peak of the SBS to a peak area which only belongs to the characteristic infrared absorption peak of matrix asphalt on the transmittance spectrum; performing a parallel test for multiple times to determine the corresponding standard A value of the SBS modified asphalt sample; performing an infrared spectroscopic transmittance spectrum test on the SBS modified asphalt sample to be tested to obtain the transmittance spectrum of the sample; computing the relative ratio of the areas of the corresponding absorption peaks of the sample; and comparing the relative ratio with the standard A value to determine the SBS content of the sample. The general infrared transmittance spectrum test technique is adopted, so the method has the advantages of simple sampling process, convenient and quick establishment of a measuring method, correct and credible quantitative result, high sensitivity, high repeatability and suitability for wide application.

Description

technical field [0001] The invention relates to a method for analyzing the content of SBS modifier in SBS modified asphalt, in particular to an infrared spectrum analysis method for the content of SBS modifier in modified asphalt. Background technique [0002] Thermoplastic rubber SBS is a block copolymer of styrene-butadiene-styrene, which is the most economical and effective asphalt modifier. SBS modified asphalt has good elastic recovery and high temperature characteristics, and can prevent low temperature cracking. It is a kind of modified asphalt widely used at home and abroad; SBS modified asphalt has excellent high and low temperature performance and unparalleled elasticity at high temperature. The application on graded roads and other roads can significantly improve the performance of the road surface, greatly improve the smoothness and friction coefficient of the road surface, prolong the service life of the road surface and reduce maintenance costs. [0003] Studi...

Claims

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Application Information

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IPC IPC(8): G01N21/35G01N21/3563
Inventor 单岗陈正发王江水岳林海刘清金达莱
Owner ZHEJIANG COMM CONSTR GRP CO LTD
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