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33 results about "Attenuated total reflection" patented technology

Attenuated total reflection (ATR) is a sampling technique used in conjunction with infrared spectroscopy which enables samples to be examined directly in the solid or liquid state without further preparation.

Disease risk assessment method and screening device based on multi-group student physical collaborative digital network

The invention discloses a disease risk assessment method and screening device based on a multi-group student physical collaborative digital network, and relates to the field of intelligent medical detection. In order to solve the defect that multi-omics-level system collaborative analysis and robust risk assessment are difficult to realize in the prior art, the technical scheme provided by the invention is as follows: acquiring a plasma sample, acquiring a spectral signal by adopting an attenuated total reflection Fourier transform infrared spectrum, and establishing a plasma spectrum digital information space; the method comprises the following steps: constructing a biological collaborative digital network containing four nodes of protein, lipid, saccharides and nucleic acid based on pathophysiology priori knowledge, and defining node strength, edge weight and network collaborative efficiency; a health baseline configuration file is established by using a health sample, a standardized deviation score of a to-be-tested sample is calculated, a comprehensive risk score is obtained, a disease screening result is output in combination with a machine learning model, and digital evaluation of multi-omics collaborative characteristics is realized. The method is suitable for non-invasive rapid screening and risk assessment work of neurodegenerative diseases and mental diseases.
Owner:HARBIN MEDICAL UNIVERSITY

Stone analysis method based on attenuated total reflection Fourier transform infrared spectroscopy

The invention provides a stone analysis method based on attenuated total reflection Fourier transform infrared spectroscopy. The stone analysis method comprises the following steps: S1, placing and fixing a stone sample to be detected; s2, acquiring an infrared light signal and converting the infrared light signal into original spectral data; s3, processing the original spectrum data to obtain a corrected spectrum; s4, taking the correction spectrum as input, obtaining a preliminary prediction category by using a partial least square discriminant analysis algorithm, and calculating a feature importance index of each wavenumber at the same time; s5, according to the feature importance index, using a random forest algorithm to obtain a secondary prediction category; and combining the accuracy rate of the partial least square discriminant analysis model and the accuracy rate of the random forest model to obtain a final prediction category. According to the method, an attenuated total reflection Fourier transform infrared spectroscopy (ATR-FTIR) technology is taken as a core, and an innovative thought of'pretreatment-free sample treatment + multi-algorithm collaborative analysis' is combined, so that a complete stone analysis process from sample fixation to clinical report output is constructed.
Owner:DOCTOR SHI (SHANGHAI) DIGITAL TECH CO LTD

Method for rapidly identifying types of yellow spots on surface of cigarette by using infrared spectrum

The invention discloses a method for rapidly identifying the type of yellow spots on the surface of a cigarette by using an infrared spectrum, and relates to the field of tobacco and cigarette products, and the method comprises the following steps: cutting a cigarette paper sample with yellow spots from cigarette paper of a yellow spot cigarette as a yellow spot sample; a cigarette paper sample without yellow spots is cut from the blank cigarette paper outside the yellow spot area to serve as an out-spot cigarette paper sample; the method comprises the following steps: respectively placing a yellow spot sample and an out-spot cigarette paper sample in an ATR part of an attenuated total reflection infrared spectrometer, collecting ATR-FTIR spectral data of the samples, and calculating an A value; comparing the A value of the macular sample and the A value of the out-of-spot cigarette paper sample with a database, performing auxiliary judgment by combining with the characteristic peak form, and judging the type of the macular according to a comparison result.
Owner:山西昆明烟草有限责任公司

Sample stage and microscope

The present invention provides a sample stage with a built-in pressure sensor for attenuated total reflectance (ATR) measurements, wherein a detachable plate can be smoothly attached and detached. The sample stage comprises: a stage surface member 4 having an opening 2; and a detachable plate 6 held by the stage surface member 4 so as to close the opening 2. Pressure sensors 8 are arranged on the stage surface member 4 at three locations along the edge of the opening 2, a sample is placed on the surface of the detachable plate 6, and three projections 18 are formed at positions corresponding to the pressure sensors 8 on the side surface of the plate or the rear surface of the plate. Each pressure sensor 8 is brought into a sensing state by placing the projections 18 of the detachable plate 6 on the pressure sensors 8 of the stage surface member 4, and each pressure sensor 8 is brought into a non-sensing state by placing the projections 18 on a portion 22A other than the pressure sensors among the edge of the opening 2, with the detachable plate 6 being rotated by a prescribed angle.
Owner:JASCO CORP

Adhesion preventive material

To provide an antiadhesive material having good handleability and improved long-term antiadhesive properties.SOLUTION: The present invention relates to an adhesion-preventing material comprising a fiber sheet and an oil agent attached to the fiber sheet, wherein the oil agent comprises liquid paraffin and a surfactant. In the present invention, the adhesion-preventing material preferably has a peak derived from an oil agent in the vicinity of a wave number of 2860cm-1 in analysis by Fourier-transform ultraviolet spectroscopy-total reflection measurement method. In the present invention, the surfactant preferably has intermediate water in which an exothermic peak based on low-temperature crystallization of water is observed at 0 °C or lower in a temperature rising process in differential scanning calorimetry (DSC) in a wet state.SELECTED DRAWING: None
Owner:EDUCATIONAL FOUND OF OSAKA MEDICAL & PHARMA UNIV +2

Attenuated total reflectance spectroscopy apparatus, and attenuated total reflectance spectroscopy method

An ATR apparatus includes a prism having a reflection surface, a holding unit holding a sample including a suspension on the reflection surface, and an adjustment unit adjusting a fluidal state of the sample held on the reflection surface. The adjustment unit adjusts the fluidal state of the sample to a first fluidal state in order to acquire a first detection result relating to the sample in the first fluidal state and adjusts the fluidal state of the sample to a second fluidal state in order to acquire a second detection result relating to the sample in the second fluidal state.
Owner:HAMAMATSU PHOTONICS KK

Method for testing shear modulus of polymer packaging material in curing process

The invention relates to a method for testing the shear modulus of a polymer packaging material in a curing process, which comprises the following steps of: 1, obtaining polymer conversion rate data at different moments and clear curing process temperature parameters through attenuated total reflection Fourier infrared spectrum in-situ monitoring based on setting of curing process temperature parameters; step 2, based on the curing process temperature parameters determined in the step 1, obtaining associated data of shear modulus and time through a synchronous mechanical property test; and step 3, based on the conversion rate data in the step 1, the curing process temperature parameters and the shear modulus and time associated data in the step 2, obtaining corresponding polymer shear moduli under different conversion rates through multi-scale data fusion. The method has the beneficial effects that high synchronism and accuracy are achieved, full-period mechanical characterization is achieved, and a scientific basis is provided for internal stress prediction and demolding time determination in the composite material forming process.
Owner:GUILIN UNIV OF ELECTRONIC TECH

Infrared spectrum quantitative method for trace hexafluorophosphate in polylactic acid fiber

The invention relates to the technical field of oil wastewater separation and trace testing, and discloses an infrared spectrum quantitative method for trace hexafluorophosphate in polylactic acid fiber, which comprises the following steps: firstly, pressing loose fiber into sheets, and carrying out infrared spectrum testing by adopting an attenuated total reflection mode to effectively enhance the acquisition intensity and stability of infrared signals; secondly, in a data processing stage, through accurately extracting a characteristic infrared signal of hexafluorophosphate and systematically determining an optimal baseline correction method of an internal standard peak and a characteristic peak and an integral range selection skill, on the basis of a relation between a characteristic peak area ratio and the concentration, the detection sensitivity of the method is improved; according to the method, a quantitative model conforming to the Lambert-Beer law is established, matrix interference can be eliminated to the maximum extent, the accuracy of a quantitative result is ensured, and the problem that trace hexafluorophosphate lower than 5% on the fiber surface is difficult to accurately and rapidly quantify by an existing infrared spectrum technology and the accuracy of a quantitative result is low is solved. And a standardized analysis process for effectively eliminating matrix interference is lacked.
Owner:XIJING UNIV

Water body COD (Chemical Oxygen Demand) detection method based on terahertz time-domain attenuated total reflection spectrum

The invention discloses a water body COD (Chemical Oxygen Demand) detection method based on a terahertz time-domain attenuated total reflection spectrum. The method comprises the steps of standard water sample preparation, standard spectrum acquisition, spectrum pretreatment and modeling, to-be-detected water sample detection and result calculation. A terahertz time-domain spectroscopy system collects a spectrum in an attenuated total reflection mode, and a COD quantitative analysis and prediction model is established. Full-process automatic detection is achieved, the detection repeatability error is smaller than 3%, the detection time of a single sample does not exceed 5 minutes, the problems of interference of chloride ions and suspended particles and loss of volatile organic compounds in a traditional method are effectively solved, and the method is suitable for various kinds of water with high salt, high turbidity and the like. Toxic chemical reagents are not needed in the whole process, waste liquid containing chromium and mercury is not generated, the method is green and environmentally friendly, the detection cost and waste liquid treatment cost are remarkably reduced, technical support is provided for real-time monitoring of the water environment and pollution traceability, and the method has high anti-interference capacity, high applicability and sustainable development benefits.
Owner:NAT ENERGY COAL & COKING GRP CO LTD

Quality detection method of refined PLAH composite plasticizer

PendingCN122330076ANon destructivePlasticizer
This invention discloses a quality testing method for refined PLAH composite plasticizers. By integrating Raman spectroscopy-attenuated total reflectance infrared dual-spectral fusion, simultaneous thermorheological characterization, accelerated migration micro-model testing, and a multi-dimensional index model, this method overcomes the shortcomings of existing technologies that only detect chemical content, cannot reflect functional performance, and lack rapid evaluation capabilities. This method achieves integrated and rapid detection of molecular structure matching, phase stability, migration risk, and long-term performance of refined PLAH composite plasticizers, with a total testing cycle of ≤8 hours and a correlation between the test results and actual application performance ≥0.92. This method requires no complex pretreatment and combines the advantages of both destructive and non-destructive testing, making it suitable for online quality control in industrial production, warehousing acceptance, and application performance prediction. It provides key technical support for the optimization of the refining process and quality control of composite plasticizers for bio-based polylactic acid (PLA) materials.
Owner:BEIJING INST OF TECH

Terahertz time-domain attenuated total reflection method-based solvent water content detection system and method

The application discloses a terahertz time-domain attenuated total reflection method solvent water content detection system and method, relates to the online detection field of solvent water content by means of terahertz time-domain spectroscopy technology, and comprises a terahertz time-domain detection device for emitting a terahertz signal to an ATR sensor module, receiving a terahertz total reflection signal emitted from the ATR sensor module, and transmitting the terahertz total reflection signal to a data processing terminal; a first ATR sensor module for receiving a sample solvent to be detected and performing total reflection on the terahertz signal by means of the sample solvent to be detected; a second ATR sensor module for performing total reflection on the terahertz signal by means of a standard sample solvent; a sample solvent online liquid taking device for controlling the sample solvent to be detected to flow through the first ATR sensor module; and a data processing terminal for calculating the water content of the sample solvent to be detected according to the terahertz total reflection signal. The application can perform online nondestructive detection on the water content of a solvent.
Owner:SOUTHWEAT UNIV OF SCI & TECH

Use of ir spectroscopy in assessing the penetration of reagents into biological specimens

Devices and associated methods and apparatus for measuring sample material (e.g., tissue samples) use involve a spectroscopic system or device configured with a sample measurement device (e.g., an attenuated total reflectance infrared (ATR-IR) sample measurement device) that includes a crystal defining a sample receiving surface / interface that is operatively connected to an IR source and an IR detector. The sample receiving surface / interface facilitates the assessment of whether a fixative (e.g., formaldehyde) (and optionally, the amount thereof) is present in a sample material, such as a tissue sample. Measurements are taken at one or more locations within a sample placement structure / region, which can be provided in the form of a probe or raised piercing structure containing one or more ATR-IR (or other) sample measurement devices. The probe can include a piercing structure or mechanism at a distal (open) end of the probe that is configured to form a channel into a selected location (depth) within the sample material in a minimally invasive manner so that the sample is not severely damaged during testing.
Owner:SAKURA FINETEK USA INC

Liquid pool for attenuated total reflection accessory of infrared spectrometer

The utility model relates to the field of infrared detection, in particular to a liquid pool for an attenuated total reflection accessory of an infrared spectrometer, which comprises a liquid bin, a liquid inlet joint, a liquid outlet joint, a first liquid inlet pipe and a first liquid outlet pipe, a first internal thread groove and a second internal thread groove are formed in the outer side wall of the liquid bin and communicated with an inner cavity of the liquid bin, a first through hole is formed in the liquid inlet connector, a second through hole is formed in the liquid drainage connector, external threads are arranged on the outer walls of the liquid inlet connector and the liquid drainage connector around the through holes, and the first liquid inlet pipe is installed in the first through hole. The first liquid discharge pipe is mounted in the second through hole; the liquid inlet connector is in threaded connection with the first inner threaded groove, the first liquid inlet pipe is communicated with an inner cavity of the liquid bin, the liquid drainage connector is in threaded connection with the second inner threaded groove, and the first liquid drainage pipe is communicated with the inner cavity of the liquid bin. The liquid inlet connector and the liquid outlet connector are in threaded connection with the two internal thread grooves respectively, so that the liquid inlet pipe and the liquid outlet pipe can be easily detached, and maintenance and replacement are facilitated.
Owner:SICHUAN JIEYUN MEDICAL TECH CO LTD

A pentazolium lead complex, its preparation method and application

This invention provides a pentaazole lead complex, its preparation method, and its application, relating to the field of laser-initiated ignition technology. The molecular formula of the pentaazole lead complex is Pb(N5)(N3), and its characterization is as follows: decomposition peak temperature: 120℃; characteristic wavenumbers detected by attenuated total reflectance infrared spectroscopy are: 3369.11, 3330.71, 3258.58, 3170.41, 1986.73, 1601.30, 1214.97 cm⁻¹. ‑1 The characteristic wavenumbers detected by Raman spectroscopy excited by 785 nm near-infrared laser are: 226.17, 573.48, 1184.74, 1342.18, and 1481.11 cm⁻¹. ‑1 Elemental analysis: PbN8: calcd N 35.10%, Found: N 35.15%. This invention discloses a novel pentazolium lead complex Pb(N5)(N3) and its preparation method. It has a low laser initiation threshold, is environmentally friendly, and experimentally determined to be successfully initiated at excitation energies of 3–100 mJ. The pentazolium lead complex described in this application does not contain ClO4. ‑ The pentazolium lead complex described in this application has higher energy than the conventional initiating explosive lead azide (Pb(N3)2), and can use a smaller amount of explosive under the same conditions.
Owner:NANJING UNIV OF SCI & TECH

Method for rapid detection of nutrient content of high-nitrogen synergistic fertilizer

PendingCN122505845AEnhance analytical certaintyAvoid cumulative errors in multi-level operationsPhysical chemistryTotal nitrogen
The present application relates to the technical field of solution physicochemical test, and discloses a method for rapidly detecting nutrient content of synergistic high-nitrogen fertilizer, comprising the following steps: collecting undiluted original solution to construct an absorbance curve by attenuated total reflectance infrared spectroscopy, reading an initial transmittance voltage value, calculating a first-order time differential to extract a change rate parameter and adjusting a time window span in combination with a voltage value drift, calculating a second-order time differential and triggering filtering according to zero-crossing to correct the parameter and determine a slope mutation point value, and inputting the corrected parameter and the voltage value into an inversion relationship to calculate and output total nitrogen nutrient content, wherein the present application separates overlapping spectra by non-equilibrium dipole polarization time sequence difference, eliminates non-linear saturation, suppresses scattering interference of incompletely dissolved particles, and improves detection accuracy.
Owner:JILIN WOYIJIA ECOLOGICAL AGRI CO LTD

Attenuated total reflection spectroscopy device and attenuated total reflection spectroscopy method

This ATR device is equipped with: a prism having a reflecting surface; a holding part that holds a sample containing a suspension on the reflecting surface; and an adjusting part that adjusts the flow state of the sample held on the reflecting surface. The adjusting part adjusts the flow state of the sample to a first flow state in order to acquire a first detection result relating to the sample in the first flow state, and adjusts the flow state of the sample to a second flow state in order to acquire a second detection result relating to the sample in the second flow state.
Owner:HAMAMATSU PHOTONICS KK

Method for evaluating desulfurization degree of bio-desulfurized rubber powder for modified asphalt

The present application relates to the technical field of road engineering, in particular to a desulfurization degree evaluation method of bio-desulfurized rubber powder for modified asphalt, which comprises Fourier infrared spectrum attenuated total reflection testing and EA element analysis testing on waste tire rubber powder and bio-desulfurized rubber powder, baseline calibration and smoothing processing on the transmittance spectrum, calculation of S-S bond and C-S bond correction peak area reduction rate, and calculation of S element content reduction rate, so as to calculate the desulfurization degree index DI value, which can quickly evaluate the desulfurization degree of bio-desulfurized rubber powder. The evaluation method and evaluation index proposed by the present application have the characteristics of short time consumption, convenient operation and high precision, can realize quick and accurate evaluation of the desulfurization degree of bio-desulfurized rubber powder in the screening stage of preparing desulfurized rubber powder modified asphalt materials, and can appropriately predict the physical properties of modified asphalt prepared by desulfurized rubber powder.
Owner:HUAZHONG UNIV OF SCI & TECH

Laminated polyester film, laminated ceramic chip capacitor, and polyester film production method

To provide a laminated polyester film which has high recyclability and excellent quality stability.SOLUTION: A laminated polyester film has a water-soluble resin layer X containing acryl having a repeating unit represented by chemical formula (1) or chemical formula (2) as a main skeleton, on at least one surface of the polyester film, and satisfies the following (1) and (2). (1) An orientation parameter Rxy of a layer X represented by Expression Rxy=(Ax-Ay) / (Ax+Ay), which is measured by total reflection measurement Fourier transform infrared spectroscopy (FT-IR-ATR), is 0.02 or more and less than 1.00. Ax: absorption intensity in a direction with maximum CH deformation vibration. Ay: absorption intensity in a direction +90° from the maximum direction. (2) A hydrophilicity parameter Wx of a layer X represented by Expression Wx=Aph / Apb, which is measured by total reflection measurement Fourier transform infrared spectroscopy (FT-IR-ATR), is 2 or more and 10 or less. Aph: area of a peak derived from a hydrophilic group at 3,000 cm-1 to 3,600 cm-1. Apb: area of a peak of CH deformation vibration of a CH2 group at 1,446 cm-1.SELECTED DRAWING: None
Owner:TORAY INDUSTRIES INC

Method for measuring molecular contents of H2O, HDO and D2O in heavy water through attenuated total reflection infrared absorption spectrum

The invention relates to a method for measuring the molecular content of H2O, HDO and D2O in heavy water by using an attenuated total reflection infrared absorption spectrum, which comprises the following steps: assembling a device comprising a Fourier transform infrared spectrometer and an ATR (Attenuated Transform Resonance) component, enabling interference light to pass through a reflecting lens to a crystal, and reflecting to a detector after total reflection; preparing a series of initial concentration heavy water solution standard samples; standing or heating the standard sample to isotope exchange equilibrium, and calculating theoretical concentration; testing the standard sample to obtain the characteristic peak areas of 1640 cm <-1 > (H2O), 1200 cm <-1 > (D2O) and 2500 cm <-1 > (O-D), and making a standard curve; and testing a blind sample and substituting into the curve to obtain the content. According to the method, the problems that the O-H peak of the high-concentration water sample is saturated and the molecular morphology of HDO and D2O cannot be distinguished in the traditional infrared spectroscopy are solved, accurate quantification is realized, and a reliable molecular level detection means is provided for the fields of nuclear industry and the like.
Owner:SHANGHAI INSTITUTE OF APPLIED PHYSICS CHINESE ACADEMY OF SCIENCES

Reaction tank and system for magnetic field electrochemical in-situ infrared spectrum test

The invention relates to the technical field of electrochemistry, and provides a reaction tank and system for a magnetic field electrochemical in-situ infrared spectrum test. The reaction tank for the magnetic field electrochemical in-situ infrared spectrum test comprises a reaction tank module, an attenuated total reflection crystal module, an electrode and gas-liquid circulation module and a magnet module, and the magnet module is configured to adjust the magnetic field intensity of a working electrode; the reaction tank main body is communicated with the opposite tank main body through an ion exchange membrane, and the main direction of ion migration on the ion exchange membrane is set to be parallel to the direction of a magnetic field applied by the magnet module. Through the magnetic field intensity adjustable magnet module, accurate and controllable application of a magnetic field on the surface of a catalyst is realized, the influence of magnetic field Lorentz force on a key ion transmission process can be eliminated under a double-cell structure, and optical path stability and magnetic field uniformity are optimized for in-situ infrared spectrum testing. Therefore, the research difficulty of electrocatalytic reaction in-situ infrared characterization in a magnetic field environment is reduced.
Owner:INST OF HIGH ENERGY PHYSICS CHINESE ACAD OF SCI

Attenuated total reflection based measurement of refractive index and carbon dioxide concentration

Systems and methods presented herein generally relate to a tool for determining a refractive index of a formation fluid using attenuated total reflection. The tool includes a body having a fluid admitting assembly and a flow line that receives the formation fluid. The tool also includes two different crystals having faces in contact with fluid in the flow line. The tool further includes at least one light source coupled to the crystals and configured to direct light into the crystals. In addition, the wavelength, the refractive indices, and the angles of incidence are configured such that the light undergoes total internal reflection at interfaces between the crystals and the formation fluid. The tool also includes at least one light detector coupled to the crystals and configured to measure reflected light exiting the crystals. The tool further includes at least one processor coupled to the at least one light detector.
Owner:SCHLUMBERGER TECH CORP

Non-specific reaction inhibitor, method for using non-specific reaction inhibitor, method for inhibiting non-specific reaction, biochemical measurement reagent, specimen pretreatment solution, and biochemical measurement reagent kit

A non-specific reaction inhibitor, which is a copolymer comprising a constitutional unit A derived from 2-methacryloyloxyethyl phosphorylcholine and exhibiting a specific physical property X measured by Fourier transform infrared spectroscopy according to an attenuated total reflection method (ATR method), the non-specific reaction inhibitor being used in a use application of inhibiting a non-specific reaction when measuring an antibody or an antigen contained in a biological sample by mixing the copolymer with the biological sample.
Owner:SEKISUI MEDICAL CO LTD

Optical module, set of optical modules, method of designing an optical module, and method of performing spectroscopy

The disclosure relates to optical modules for spectroscopy. In one arrangement, a transmission body (4) is provided that defines a sensing surface (10) configured to contact a sample (8) during a spectroscopic measurement of the sample (8) by attenuated total reflection using optical radiation (13). The sensing surface (10) comprises a meta-surface structure (16) configured to apply a wavelength-selective enhancement of absorption of the radiation (13) by the sample (8) during the measurement.
Owner:UNIV OF SOUTHAMPTON

Attenuated total reflectance spectroscopy apparatus, and attenuated total reflectance spectroscopy method

This ATR device is equipped with: a prism having a reflecting surface; a holding part that holds a sample containing a suspension on the reflecting surface; and an adjusting part that adjusts the flow
Owner:HAMAMATSU PHOTONICS KK

Method and device for identifying common plastics

The invention provides a method and a device for identifying common plastics. The method comprises the following steps: measuring an intermediate infrared spectrum of a sample to be identified by using an attenuated total reflection Fourier transform infrared spectroscopy (ATR-FTIR); intercepting a characteristic wave band of the intermediate infrared spectrum, dividing the characteristic wave band into a plurality of equal-length sub-intervals, and performing two-dimensional reconstruction on the plurality of equal-length sub-intervals to obtain a two-dimensional data matrix; and inputting the two-dimensional data matrix into a pre-established two-dimensional convolutional neural network (CNN2D) model to obtain the plastic category of the sample to be identified. According to the invention, common plastic types can be quickly identified, secondary pollution is avoided, the efficiency is high, the speed is high, the identification accuracy rate is high, and the classification accuracy rate is high.
Owner:CHINA PETROLEUM & CHEMICAL CORP +1

Resin film, metal-clad laminate, and method for producing resin film

The purpose of the present invention is to provide a resin film which is less likely to undergo blocking even when stored in a roll-like form for a long period of time. Provided is a long resin film containing at least a fluororesin. On at least one surface of the resin film, the ratio A2 / A1 of the absorbance A2 of a second peak to the absorbance A1 of a first peak is 0.006 or less when measured by infrared spectroscopy attenuated total reflection method (IR-ATR), wherein the first peak is a peak of CF2 symmetric stretching vibration in the wavenumber range of 1130 cm-1 to 1180 cm-1 inclusive and the second peak is a maximum peak in the wavenumber range of 1700 cm-1 to 1750 cm-1 inclusive. The ratio N2/N1 of the absorbance N2 of a fourth peak to the absorbance N1 of a third peak is 0.05 to 0.5 inclusive when measured by nano-infrared spectroscopy (nano-IR), wherein the third peak is a peak of CF2 symmetric stretching vibration in the wavenumber range of 1130 cm-1 to 1180 cm-1 inclusive and the fourth peak is a maximum peak in the wavenumber range of 1600 cm-1 to 1800 cm-1 inclusive. The average value of water contact angles is 55° to 105° inclusive, and the variation coefficient of the water contact angles is 30% or less.
Owner:DAIKIN INDUSTRIES LTD

Electrode and secondary battery including same

The present specification relates to an electrode comprising: an electrode laminate film including an active material and a binder that has a three-dimensional fiber network structure; and a current collector having at least one surface on which the electrode laminate film is disposed. In the electrode, a high-intensity region accounts for 4.5% to 48.0% of the total surface area. The high-intensity region is defined as a region in which the intensity (IB) of a peak appearing in a wavenumber range of 1190 cm-1 to 1260 cm-1 in an IR spectrum derived by analyzing a surface of the electrode using attenuated total reflectance Fourier transform infrared spectroscopy (ATR-FTIR) is 1.5 or higher. As a result, it is possible to provide an electrode in which structural features such as the fiber thickness, the fiber content, and the arrangement state of the fibrous binder on the electrode surface are controlled, and which thus has excellent appearance and resistance characteristics. In addition, it is possible to provide a secondary battery, a battery box, and an electrical device having excellent durability and lifespan properties as well as excellent output and rapid charging performance.
Owner:LG ENERGY SOLUTION LTD

Sample stage and microscope

The present invention provides a sample stage with a built-in pressure sensor compatible with attenuated total reflection (ATR) measurements, which allows for smooth attachment and detachment of the detachable plate. The sample stage includes a stage surface member 4 having an opening 2 and a detachable plate 6 held by the stage surface member 4 so as to cover the opening 2. Pressure sensors 8 are arranged on the stage surface member 4 at three locations along the edge of the opening 2. A sample is placed on the surface of the detachable plate 6, and three protrusions 18 are formed on the side or back of the plate at positions corresponding to the pressure sensors 8. Placing the protrusions 18 of the detachable plate 6 on the pressure sensors 8 of the stage surface member 4 places the pressure sensors 8 in a sensing state. Rotating the detachable plate 6 by a predetermined angle and placing the protrusions 18 on a portion 22A of the edge of the opening 2 other than the pressure sensors places the pressure sensors 8 in a non-sensing state.
Owner:JASCO CORP

Electrode and secondary battery comprising same

The present specification relates to an electrode comprising: an electrode mixture film including an electrode active material and a binder having a three-dimensional fiber network structure; and a current collector having the electrode mixture film disposed on at least one surface thereof, wherein the electrode has a low-intensity region of 15.0% or more on the basis of area with respect to the entire region on the surface thereof, and the low-intensity region is defined as a region in which IB, the intensity of a peak appearing in the range of wave numbers of 1190 cm-1 to 1260 cm-1, is 1.0 or less in an IR spectrum derived by analyzing the surface of the electrode by attenuated total reflection infrared spectroscopy (ATR-FTIR). Through this, structural characteristics such as fiber thickness, fiber amount, and arrangement state of the fibrous binder on the electrode surface are controlled, so that calendering processability is excellently performed, thereby providing an electrode having excellent appearance characteristics, and providing a secondary battery, a battery box, and an electric device having excellent durability, lifespan characteristics, output, and rapid charging performance.
Owner:LG ENERGY SOLUTION LTD

In-situ attenuated total reflection Fourier transform infrared spectrum detection method based on microwave heating

The invention discloses an in-situ attenuated total reflection Fourier transform infrared spectrum detection method based on microwave heating, and belongs to the technical field of spectrum detection and analysis. According to the method, a design strategy that microwave heating and an infrared spectrum system are arranged separately is adopted, and a high-refractive-index infrared reflection crystal is used as a unique coupling detection area, so that real-time infrared spectrum monitoring of a reaction system is realized. The detection method disclosed by the invention is particularly suitable for in-situ monitoring of hydrogenation, cracking and conversion reaction of an oxygen-containing or unsaturated substituent compound on a furan ring or a benzene ring, and is compatible with microwave and catalytic reaction mechanism research, material interface reaction analysis and spectroscopic characterization of a biomass derivative conversion process; the method has the advantages of being accurate in temperature control, high in response speed, high in signal stability and good in data repeatability, dynamic spectrum tracking can be conducted on a complex reaction system, a traditional external heating detection mode is compatible, and the space matching degree and the time resolution of microwave field in-situ characterization are remarkably improved.
Owner:INST OF CHEM IND OF FOREST PROD CHINESE ACAD OF FORESTRY