Acrylic resin emulsion for fingerprint-resistant paint and preparation method thereof

An acrylic resin and anti-fingerprint technology, applied in antifouling/underwater coatings, coatings, paints containing biocides, etc., can solve the problems of sticking rolls and poor curing, poor high temperature resistance of coatings, etc., to achieve size matching, Good stability and uniform system

Inactive Publication Date: 2013-04-24
江苏巨珩新材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The acrylic resin should have a certain glass transition temperature, the low glass transition temperature makes the coating poor in high temperature resistance, sticking to the roller and poor curing in the continuous production of coating

Method used

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  • Acrylic resin emulsion for fingerprint-resistant paint and preparation method thereof

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0050] An acrylic resin emulsion for fingerprint-resistant coatings, calculated in parts by weight, composed of the following components through reaction polymerization:

[0051] 35 parts of methyl methacrylate;

[0052] 10 parts of methyl acrylate;

[0053] 30 parts of ethyl methacrylate;

[0054] 15 parts of acrylic acid;

[0055] 0.1 part of azobisisobutyronitrile;

[0056] 3 copies of OP-10;

[0057] 12 parts of ethylene glycol butyl ether;

[0058] 150 parts of deionized water.

[0059] The preparation method includes the following steps:

[0060] (1) Add OP-10, water, ethylene glycol butyl ether, and azobisisobutyronitrile into the reaction kettle, stir, and raise the temperature to 80°C;

[0061] (2) Mix methyl methacrylate, methyl acrylate, ethyl methacrylate and acrylic acid uniformly to form a monomer mixture, and add the monomer mixture dropwise to the reactor;

[0062] (3) 75℃, heat preservation for 1.5 hours;

[0063] (4) Filter out the material;

[0064] (5) Dilute with water to 30...

Embodiment 2

[0066] An acrylic resin emulsion for fingerprint-resistant coatings, calculated in parts by weight, composed of the following components through reaction polymerization:

[0067] 40 parts of methyl methacrylate;

[0068] 5 parts of methyl acrylate;

[0069] 35 parts of ethyl methacrylate;

[0070] 10 parts of acrylic acid;

[0071] 0.2 parts of azobisisobutyronitrile;

[0072] 1 copy of OP-10;

[0073] 1 part of sodium lauryl sulfate;

[0074] 8 parts of ethylene glycol butyl ether;

[0075] 200 parts of deionized water.

[0076] The preparation method includes the following steps:

[0077] (1) Add OP-10, sodium lauryl sulfate, water, ethylene glycol butyl ether, and azobisisobutyronitrile into the reaction kettle, stir, and heat to 70°C;

[0078] (2) Mix methyl methacrylate, methyl acrylate, ethyl methacrylate and acrylic acid uniformly to form a monomer mixture, and add the monomer mixture dropwise to the reactor;

[0079] (3) 80°C, heat preservation for 2 hours;

[0080] (4) Filter out the ma...

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Abstract

The invention discloses an acrylic resin emulsion for fingerprint-resistant paint and a preparation method thereof. The acrylic resin emulsion for fingerprint-resistant pain is polymerized from the following components in parts by weight:35-40 parts of methyl methacrylate, 5-10 parts of methyl acrylate, 30-35 parts of ethyl methacrylate, 10-15 parts of acrylic acid, 0.1-0.2 part of initiator, 2-4parts of emulsifying agent, 8-12 parts of cosolvent and 150-200 parts of deionized water. The acrylic resin emulsion has the advantages of uniform system, uniform viscosity and favorable ionic stability, and can satisfy the requirement of quick curing without degrading the film-forming properties of the resin. When the fingerprint-resistant paint prepared from the acrylic resin emulsion is coatedon the surface of a galvanized steel sheet, fingerprints can not be attached to the surface, and the paint is environment-friendly.

Description

Technical field [0001] The invention relates to an acrylic resin emulsion and a preparation method thereof, in particular to an acrylic resin emulsion for fingerprint resistant coatings and a preparation method thereof. Background technique [0002] As an environmentally friendly coating, water-based resin is one of the current hot spots in the research and development of coatings. There are three ways to make the resin water-based: (1) make the resin salt and dissolve in water (2) use the -OH or ether bond in the resin skeleton Hydrophilic genes make the resin soluble in water (3) rely on surfactants to solubilize and dissolve in water. The first two methods are mainly used to manufacture water-based coatings, and the latter method is mainly used to make emulsions. Therefore, the first two methods are generally two-component water-based resins, which require a certain amount of curing agent and catalyst to be added to the coating to accelerate The coating film is dried, and the...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08F220/14C08F220/18C08F220/06C08F2/26C09D133/12C09D5/16
Inventor 周筱祯汪茂军
Owner 江苏巨珩新材料科技有限公司
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