Dispersing agent for positive and negative electrode materials of lithium ion battery
A lithium-ion battery and dispersant technology, which is applied in the direction of battery electrodes, circuits, electrical components, etc., can solve the problem of affecting the energy density of the battery to improve the application of lithium-ion batteries, can not significantly improve the electrochemical performance of the battery, and the battery performance cannot be fully utilized To avoid the replacement of preparation process and equipment, improve the safety test, and shorten the dispersion time
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[0026] 1. Preparation of dispersant:
[0027] (1) Preparation of polyoxyethylene ether
[0028] Weigh 20kg of polyvinyl alcohol into a 100L stainless steel reaction kettle, and at the same time weigh 10kg of toluene or other less polar solvents into the reaction kettle as a primer solvent. Close the feeding port with nitrogen (N 2 ) (494kPa) for 3 times to get rid of the air in the kettle, and at the same time start to heat up to 110°C-120°C, vacuum 2-3 times for vacuum dehydration, the time is about 10min, and then fill the kettle with nitrogen (N 2 ) to slightly higher than normal pressure. Add analytically pure caustic soda (NaOH) or caustic soda (KOH), and feed an appropriate amount of dehydrated ethylene oxide gas until the amount of feed reaches the predetermined requirement. During this period, it is necessary to cool the volatilized reflux toluene and carry out an oil-water separator to remove a small amount of water generated in the reaction, and to control the mol...
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