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Method for preparing edible idesia oil

A technology of sycamore oil and sycamore, which is applied in the field of preparation of edible sycamore oil, can solve the problems of reducing health care nutritional value, affecting the quality of oil and fat, large amount of excess alkali, etc., and achieves stable properties, short production cycle, and finished oil fume. high point effect

Inactive Publication Date: 2011-09-21
SICHUAN ACAD OF FORESTRY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the high acid value of oil, the amount of excess alkali added in the chemical alkali refining process is large, and the alkali also saponifies a large amount of neutral oil during the neutralization process with free fatty acids, resulting in a low refining yield; physical refining water vapor For deacidification, the oil needs to be treated at high temperature for a long time, which affects the quality of the oil. Some active ingredients in the oil, such as VE and sterol, will overflow with the steam stripping, reducing the nutritional value of health care

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] (1), pretreatment

[0028] Filter the jatropha crude oil with a filter cloth to remove mechanical impurities;

[0029] (2), degumming

[0030] Put 100 parts of the pretreated jatropha oil into a three-necked flask, add 0.5 parts of phosphoric acid with oil weight at a temperature of 75 ° C, stir for 20 minutes, and centrifuge the lower layer of gum after cooling, and wash the upper layer of jatropha oil with deionized water To neutral, to obtain jatropha degummed oil;

[0031] (3), dehydration

[0032] Dehydrate the above degummed oil at a vacuum degree of 4000Pa and a temperature of 60°C for 30min;

[0033] (4), deacidification

[0034] 100 parts of the above dehydrated oil were continuously deacidified at a temperature of 105°C, a pressure of 10Pa, a feed rate of 80mL / h, and a wiper speed of 150r / min.

Embodiment 2

[0036] (1), pretreatment

[0037] Filter the jatropha crude oil with a filter cloth to remove mechanical impurities;

[0038] (2), degumming

[0039] Put 100 parts of the pretreated jatropha oil into a three-necked flask, add 2.0 parts of phosphoric acid with oil weight at a temperature of 80°C, stir for 35 minutes, and centrifuge the lower layer of gum after cooling, and wash the upper layer of jatropha oil with deionized water To neutral, to obtain jatropha degummed oil;

[0040] (3), dehydration

[0041] Dehydrate the above degummed oil at a vacuum degree of 5000Pa and a temperature of 60°C for 20min;

[0042] (4), deacidification

[0043] 100 parts of the above-mentioned dehydrated oil were continuously deacidified at a temperature of 130°C, a pressure of 20 Pa, a feed rate of 120mL / h, and a wiper speed of 200r / min.

Embodiment 3

[0045] (1), pretreatment

[0046] Filter the jatropha crude oil with a filter cloth to remove mechanical impurities;

[0047] (2), degumming

[0048] Put 100 parts of the pretreated jatropha oil into a three-necked flask, add 1.5 parts of phosphoric acid with oil weight at a temperature of 77°C, stir for 25 minutes, and centrifuge the lower layer of gum after cooling, and wash the upper layer of jatropha oil with deionized water To neutral, to obtain jatropha degummed oil;

[0049] (3), dehydration

[0050] Dehydrate the above degummed oil at a vacuum degree of 4500Pa and a temperature of 75°C for 25min;

[0051] (4), deacidification

[0052] 100 parts of the above-mentioned dehydrated oil were continuously deacidified at a temperature of 110°C, a pressure of 15 Pa, a feed rate of 100mL / h, and a speed of 170r / min of the wiper.

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PUM

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Abstract

The invention discloses a method for preparing idesia oil, which is characterized by comprising the following steps of: filtering crude idesia oil by a filtering cloth to remove mechanical impurities; adding 100 parts of the filtered crude idesia oil into 0.5 to 2.0 parts of degumming agents at 75 to 80 DEG C; stirring for 20 to 35 minutes; cooling and centrifuging to separate the colloid in the lower layer; washing the idesia oil in the upper layer by using deionized water to a neutral state to obtain degummed idesia oil; dehydrating the degummed idesia oil at a vacuum degree of 4000 to 5000 Pa and the temperature of 60 to 80 DEC C for 20 to 30 minutes; continuously deacidifying the dehydrated idesia oil at the temperature of 105 to 130 DEG C, the pressure of 10 to 20 Pa, the feed rate of 80 to 120 mL / h and the film scraper rotation speed of 150 to 200 r / min, wherein the light component is removed free fatty acid, and the heavy component is product oil. The method has the advantages that the colloid and the fatty acid are removed completely, the production period is short, the effective ingredients, such as vitamin E and the like in the grease are effectively remained; the prepared edible idesia oil has the advantages of high yield, high smoke point, stable property in a storage process, no precipitate, and invariant color; and a special deodorization technology is not needed.

Description

technical field [0001] The invention relates to a preparation method of edible jatropha oil, belonging to the technical field of edible oil processing. Background technique [0002] Idesia polycarpa Maxim.var.vestita Diels is a plant of the genus Idesia polycarpa Maxim.var.vestita Diels, a deciduous tree, distributed in the Yangtze River Basin of my country, especially in Sichuan, Shaanxi and other places where there are a large number of wild resources. The oil content of jacaranda is as high as 36-38%, the oil yield per plant is as high as 25-30kg, and the production period is as long as 40-50 years. Carapacea oil is rich in unsaturated fatty acids and has high nutritional value. Early research and the actual consumption process of local farmers in the producing area have also proved its safety. In addition, my country has a large population and little arable land, so the cultivation of jacaranda does not occupy arable land. Making full use of jacaranda resources is condu...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B3/00C11B3/04A23D9/04
Inventor 吴斌张正香付卓锐莫开林
Owner SICHUAN ACAD OF FORESTRY
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