Natural antifungal textile containing tangerine peel extract and manufacturing method thereof
A tangerine peel extract and antifungal technology applied in the field of textiles to achieve strong antibacterial activity, simple preparation process, and good antibacterial rate
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Embodiment 1
[0018] Embodiment 1 A kind of preparation method of the natural antifungal textile containing tangerine peel extract
[0019] (1) Preparation of microcapsules: Weigh 10 parts of tangerine peel extract, 1 part of polyvinyl alcohol, 30 parts of glutaraldehyde, and 2 parts of emulsifier, mix the tangerine peel extract and polyvinyl alcohol aqueous solution, mix well and inject 1 part of The continuous phase of the emulsifier is emulsified in n-hexane at a high speed, and the rotation speed is 700r / min to prepare emulsion A; mix glutaraldehyde with 5 drops of 10% hydrochloric acid aqueous solution, mix well and inject another part of the continuous phase n-hexane containing 1 part of emulsifier High-speed emulsification in alkanes, rotating speed 700, to prepare emulsion B; mix the two emulsions A and B at 10°C, and stir at high speed for 0.5h, filter, wash with petroleum ether for 3 times, and freeze-dry at -10°C to obtain microcapsules;
[0020] (2) Use the printing method to fi...
Embodiment 2
[0028] Embodiment 2 A kind of preparation method of the natural antifungal textile containing tangerine peel extract
[0029] (1) Preparation of microcapsules: Weigh 30 parts of tangerine peel extract, 10 parts of polyvinyl alcohol, 60 parts of glutaraldehyde, and 30 parts of emulsifier, mix the tangerine peel extract and polyvinyl alcohol aqueous solution, mix well and inject 15 parts of The continuous phase of the emulsifier is emulsified in n-hexane at a high speed and the rotation speed is 2500r / min to prepare emulsion A; mix glutaraldehyde with 10 drops of 30% hydrochloric acid aqueous solution, mix well and inject another part of the continuous phase n-hexane containing 15 parts of emulsifier Emulsion B was prepared by high-speed emulsification in alkanes at a speed of 2500r / min; the two emulsions A and B were mixed at 30°C, stirred at high speed for 2 hours, filtered, washed 5 times with petroleum ether, and freeze-dried at -5°C to obtain microcapsules;
[0030] (2) Use...
Embodiment 3
[0038] Embodiment 3 A kind of preparation method of the natural antifungal textile containing tangerine peel extract
[0039] (1) Preparation of microcapsules: Weigh 20 parts of tangerine peel extract, 5 parts of polyvinyl alcohol, 40 parts of glutaraldehyde, and 20 parts of emulsifier, mix the tangerine peel extract and polyvinyl alcohol aqueous solution, mix well and inject 10 parts of The continuous phase of the emulsifier is emulsified in n-hexane at a high speed and the rotation speed is 2000r / min to prepare emulsion A; mix glutaraldehyde with 7 drops of 20% hydrochloric acid aqueous solution, mix well and inject another continuous phase n-hexane containing 10 parts of emulsifier Emulsion B was prepared by high-speed emulsification in alkanes at a speed of 2000r / min; the two emulsions A and B were mixed at 20°C, stirred at high speed for 1 hour, filtered, washed 4 times with petroleum ether, and freeze-dried at -8°C to obtain microcapsules;
[0040] (2) Fix the microcapsu...
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