Detection method for cross section of fiber

A detection method and fiber cross-section technology, which is applied in the field of fiber cross-section detection, can solve the problems of affecting the fiber, reducing the reliability of observation, and it is difficult to obtain all the information of the fiber at one time, so as to achieve the effect of improving the accuracy rate

Inactive Publication Date: 2012-04-04
DONGHUA UNIV +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the diameter of the fiber can generally reach tens of microns, which is greater than the depth of field of the microscope, so it is difficult to obtain all the information of the fiber cross section at one time.
At the same time, due to the limited size of the microscope lens, it is necessary to move and observe a large area of ​​the sample many times, so the reliability of the observation is also greatly reduced
In addition, for fibers such as dyeing, additional information on the surface will seriously affect the performance of the fiber itself

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] (1) Detection of the longitudinal section of the fiber: the fiber is placed flat on the gelatin film, then the fiber and the gelatin film are clamped in the middle with two metal plates, and after the above-mentioned two metal plates are fixed (two metal plates The force between the plates is 1.5bar), heated to 100°C for drying, and the drying time is 30min. After heating, put it into the refrigerator to cool; finally, the fibers are removed from the gelatin film, and the gelatin film Obtain the imprint map of the longitudinal section of the fiber;

[0021] (2) Detection of fiber cross-section: stick the fiber to the bottom of the container with a starch adhesive, and then add the resin mixture (polyester resin 98-99%, benzoyl peroxide 2-1%) in the container, Then heat to 70°C and dry for 60 minutes to polymerize the resin mixture, and after cooling at room temperature, cut out slices with a thickness of 12 μm, and finally glue the obtained slices on glass slides and pu...

Embodiment 2

[0023] (1) Detection of fiber longitudinal section: place the fiber flat on the polystyrene film, then sandwich the fiber and the polystyrene film with two metal plates, and fix the above two metal plates (the force between the two metal plates is 2.0bar), heated to 100~125°C for drying, the drying time is 15~30min, after heating, put it into cooling device to cool immediately; After removing it from the styrene film, the imprint map of the longitudinal section of the fiber can be obtained on the polystyrene film;

[0024] (2) Detection of fiber cross-section: use adhesive to stick the fiber to the bottom of the carton with a side length of 40-60mm, then add the resin mixture into the carton, and then heat to 80°C to dry, the drying time is 40min, Polymerize the resin mixture and cool it at room temperature, cut out slices with a thickness of 18 μm, and finally glue the obtained slices on a glass slide and put them in cedar oil for microscope observation.

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Abstract

The invention relates to a detection method for the cross section of a fiber. The detection method comprises the following steps: 1, horizontally laying the fiber on a film, sticking two metal plates between the fiber and the film, fixing the two metal plates, drying, cooling, carrying down the fiber from the film to obtain an impression picture of the longitudinal cross section of the fiber on the film; and 2, adhering the fiber to the bottom of a container by an adhesive, adding a resin mixture to the container, drying to polymerize the resin mixture, cooling at room temperature, slicing toobtain a slice, adhering the slice to a slide glass, and putting the slide glass in cedar oil for the microscope observation. The detection method of the invention has the advantages of simplicity, no new equipment requirement, and realization of the large scale application. Compared with the direct microscope observation, the method of the invention allows the obtained field depth to be better, complete information of the cross section of the fiber to be once obtained, and influences of dyes of the surface of the fiber to be eliminated, so the discrimination accuracy on the fiber is improved.

Description

technical field [0001] The invention belongs to the field of fiber identification, in particular to a fiber section detection method. Background technique [0002] With the massive development of chemical fibers, there are more and more varieties of new fibers, including special fibers, composite fibers, modified fibers, etc. in addition to conventional fibers. In order to facilitate production management and product analysis, scientific identification of textile fibers is required. Fiber identification includes identification of morphological characteristics and identification of physical and chemical properties. Microscopic observation is commonly used in the identification of morphological characteristics. Using a microscope to observe the longitudinal and cross-sectional shapes of fibers is the basic method for identifying various textile fibers, and is often used to identify fiber categories. Natural fibers each have a special morphology that can be correctly identifi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/84G01N1/44
Inventor 薛文良魏孟媛韩晨晨薛剑
Owner DONGHUA UNIV
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