Method for preparing hydrocracking catalyst
A technology for hydrocracking and catalyst is applied in the field of medium oil type hydrocracking catalyst and its preparation, which can solve the problems of low catalyst activity, large surface area, catalyst loss, etc., and is beneficial to the exertion of metal activity and simplifies the preparation process. , the effect of increased lytic activity
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Embodiment 1
[0029] Put 150.7 grams of amorphous silica-alumina prepared by graft copolymerization, 55.6 grams of macroporous alumina, and 148.4 grams of binder prepared by dilute nitric acid and small-pored alumina into a roller compactor, and then rolled for 30 minutes, and then added Appropriate amount of water, grind until the paste can be extruded, extruded, and dried at 180°C for 4 hours to obtain the carrier. with WO 3 56g / 100ml, NiO12g / 100ml impregnation solution impregnated the carrier at room temperature for 2 hours, separated the mother liquor, dried at 110°C for 4 hours, and calcined at 500°C for 4 hours to obtain catalyst C1.
Embodiment 2
[0034] Put 133.4 grams of amorphous silica-alumina prepared by 150.7 grams of graft copolymerization, 28.5 grams of boric acid, 46.6 grams of macroporous alumina, and 133.4 grams of adhesives prepared by dilute nitric acid and small-pored alumina into a rolling machine, and roll for 30 Minutes, then add an appropriate amount of water, grind until the paste can be extruded, extrude, and dry the extruded strips at 150 ° C for 8 hours to obtain a carrier. with WO 3 56g / 100ml, NiO12g / 100ml impregnation solution impregnated the carrier at room temperature for 2 hours, separated the mother liquor, dried at 110°C for 4 hours, and calcined at 500°C for 4 hours to obtain catalyst C2.
Embodiment 3
[0036] Put 133.4 grams of amorphous silica-alumina prepared by 150.7 grams of graft copolymerization, 14.3 grams of boric acid, 46.6 grams of macroporous alumina, and 133.4 grams of adhesives prepared by dilute nitric acid and small-pored alumina into a rolling machine, and roll for 30 Minutes, then add an appropriate amount of water, grind until the paste can be extruded, extrude, and dry the extruded strips at 200 ° C for 6 hours to obtain a carrier. with WO 3 56g / 100ml, NiO12g / 100ml impregnation solution impregnated the carrier at room temperature for 2 hours, separated the mother liquor, dried at 110°C for 4 hours, and calcined at 500°C for 4 hours to obtain catalyst C3.
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