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Production method for shell-based carbon molecular sieve

A technology of fruit shell-based carbon and molecular sieve, which is applied in the direction of separation methods, chemical instruments and methods, and carbon compounds. It can solve the problems of unsatisfactory use effects and rough methods, and achieve ideal use benefits, long service life, and increase nitrogen production. rate effect

Active Publication Date: 2013-06-12
湖州强大分子筛科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the method for preparing carbon molecular sieves from coconut shells as a raw material is relatively rough and unsatisfactory. How to improve the existing method of preparing carbon molecular sieves using coconut shells as raw materials to effectively improve the quality of the produced carbon molecular sieves, become a problem to be solved urgently by those skilled in the art

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] Embodiment 1: a kind of preparation method of shell base carbon molecular sieve, comprises following production steps:

[0024] a. Raw material ratio; mix 60-70 parts of flower mud and 30-40 parts of coconut shell carbonized material to obtain product A; flower mud can be dry flower mud, wet flower mud (moisturizing flower mud) or flower mud leftovers ; Coconut shell carbonized material is a conventional processed product of coconut shell, which can be purchased in the market;

[0025] b. Drying: Dry product A in an oven at 100-130°C for 10-20 minutes to obtain product B;

[0026] c. Finely pulverize the product B until the diameter is 10-20nm to obtain the product C;

[0027] d. Pickling; place product C in 2-3% hydrochloric acid solution, soak for 1-2 hours, wash after soaking; then place in 2-3% hydrochloric acid solution, soak for 1-2 hours, and then carry out after soaking Washing; get D product;

[0028] e. Secondary drying: place product D in an oven at 60-80°...

Embodiment 2

[0032] Embodiment 2: a kind of preparation method of shell base carbon molecular sieve, comprises following production steps:

[0033] a. Raw material ratio; mix 65 parts of flower mud and 35 parts of coconut shell carbonized material to obtain product A; the flower mud can be dry flower mud, wet flower mud (moisturizing flower mud) or flower mud leftovers; coconut shell carbonization The material is a conventional processed product of coconut shell, which can be purchased in the market;

[0034] b. Drying: Dry product A in an oven at 120°C for 15 minutes to obtain product B;

[0035] c, finely pulverize, pulverize product B to a diameter of 15nm to obtain product C;

[0036] d, pickling; place product C in 2-3% hydrochloric acid solution, soak for 1.5 hours, wash with water after soaking; then place in 2-3% hydrochloric acid solution, soak for 1.5 hours, wash with water after soaking; get D Taste;

[0037] e. Secondary drying; place product D in an oven filled with nitroge...

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PUM

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Abstract

The invention discloses a production method for a shell-based carbon molecular sieve, which includes the production steps of a proportioning of raw materials, b drying, c fine crushing, d acid-washing, e secondary drying, f forming by extruding to strips, g high-temperature nitrogen-based carbonization and h high-temperature nitrogen-based hole-adjusting processing. The production method for the shell-based carbon molecular sieve uses coconut shells as raw materials to produce the carbon molecular sieve and achieves waste utilization of the coconut shells. Meanwhile, compared with a traditional production method for a carbon molecular sieve, the production method for the shell-based carbon molecular sieve is simple in process of production process and low in production cost and has superior performances in terms of produced nitrogen concentration, produced nitrogen amount, recovery rate, compression strength and the like.

Description

technical field [0001] The invention relates to a production method of nitrogen-making carbon molecular sieves, in particular to a preparation method of fruit shell-based carbon molecular sieves. Background technique [0002] There are a large number of coconut trees planted in the south of our country. Coconut juice and coconut meat are natural foods rich in nutrition, which can be made into coconut milk, shredded coconut, food spices, etc. But most of the coir shells of coconut fruit are discarded by people, and need a large amount of manpower, material resources and financial resources to be processed, generally carried out incineration, which will also cause environmental pollution. [0003] Carbon molecular sieve is a new type of activated carbon that almost only contains uniform micropores with a diameter of several angstroms. This pore characteristic can endow nitrogen-making carbon molecular sieve with selective adsorption performance according to its pore size and ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J20/20B01J20/30C01B31/02C01B21/04B01D53/04C01B32/306C01B32/324
Inventor 吴会荣
Owner 湖州强大分子筛科技有限公司
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