High temperature-resistant nylon/thermotropic liquid crystal polymer blend and preparation method for blend
A liquid crystal polymer, high temperature resistant technology, applied in the polymer field, can solve the problems of high price, low mechanical properties and poor fluidity of liquid crystal polymers, and achieve the effect of expanding the scope of use, overcoming poor fluidity and avoiding anisotropy
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Embodiment 1
[0034] (1) Vacuum dry 80 parts of HPN at 90°C for 24 hours for later use, and dry 10 parts of TLCP at 130°C for 4 hours for later use;
[0035] (2) Take 7 parts of compatibilizer PE-g-MAH, 0.4 part of antioxidant 1098 and 0.2 part of antioxidant 168, and 0.8 part of lubricant calcium stearate to be dried separately for use;
[0036] (3) The above-mentioned components are fully mixed in a high-speed mixer;
[0037] (4) Then put it into a twin-screw extruder for extrusion granulation. The temperature of the extruder is: Zone 1 temperature: 270°C, zone 2 temperature: 285°C, zone 3 temperature: 300°C, zone 4 temperature: 310°C, zone 5 temperature: 320°C, zone 6 temperature: 300°C, zone 7 Zone temperature: 285°C, head temperature: 175°C; extrusion rate: 180r / min, residence time: 2min.
Embodiment 2
[0039] (1) Vacuum dry 70 parts of HPN at 80°C for 24 hours for later use, and dry 10 parts of TLCP at 130°C for 4 hours for later use;
[0040] (2) Take 5 parts of compatibilizer PE-g-MAH, 0.6 part of antioxidant 1098 and 0.2 part of antioxidant 168, and 0.4 part of lubricant zinc stearate and dry them separately for use;
[0041] (3) The above-mentioned components are fully mixed in a high-speed mixer;
[0042] (4) Then put it into a twin-screw extruder for extrusion granulation. The temperature of the extruder is: Zone 1 temperature: 280°C, zone 2 temperature: 290°C, zone 3 temperature: 305°C, zone 4 temperature: 315°C, zone 5 temperature: 320°C, zone 6 temperature: 310°C, zone 7 Zone temperature: 290°C, head temperature: 180°C; extrusion rate 200r / min, residence time 1min.
Embodiment 3
[0044] (1) Vacuum dry 90 parts of HPN at 100°C for 24 hours for later use, and dry 8 parts of TLCP at 130°C for 4 hours for later use;
[0045] (2) Take 5 parts of compatibilizer PE-g-MAH, 0.7 part of antioxidant 1098 and 0.1 part of antioxidant 168, and 0.2 part of lubricant calcium stearate and dry them separately for use;
[0046] (3) The above-mentioned components are fully mixed in a high-speed mixer;
[0047] (4) Then put it into a twin-screw extruder for extrusion granulation. The temperature of the extruder is: Zone 1 temperature: 270°C, zone 2 temperature: 280°C, zone 3 temperature: 300°C, zone 4 temperature: 310°C, zone 5 temperature: 320°C, zone 6 temperature: 300°C, zone 7 Zone temperature: 285°C, head temperature: 190°C; extrusion rate 150r / min, residence time 3min.
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Abstract
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