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Potassium hexatitanate whisker heat insulating brick and production method thereof

A potassium hexatitanate whisker, thermal insulation technology, applied in the field of thermal insulation materials, can solve the problem that the thermal insulation effect of thermal insulation bricks is difficult to meet the strict requirements of industrial furnace energy-saving targets, and achieve good energy-saving effect, good thermal insulation effect, The effect of low thermal conductivity

Inactive Publication Date: 2013-08-21
BEIJING UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, the heat insulation effect of the above-mentioned insulation bricks is still difficult to meet the increasingly stringent requirements of industrial furnaces for energy-saving goals

Method used

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  • Potassium hexatitanate whisker heat insulating brick and production method thereof

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] Insulation bricks are prepared by the following process:

[0026] 1) Mix potassium hexatitanate whiskers with a length of 60-80 μm, a diameter of 0.3-0.5 μm, and an aspect ratio of 150-200, alumina and cement with a particle size of 2-5 μm, and dry-roll for 15 minutes.

[0027] 2) Then add sodium carboxymethyl cellulose, water glass and water successively, continue rolling for 25 minutes, roll out, and shape the blank in the brick-making mold.

[0028] 3) Air-dry the above-mentioned insulating brick blanks for 48 hours, then put them into the furnace for roasting, the heating rate is 60°C / h, heat up to 500°C, keep warm for 15 hours, then cool down in the furnace, when the temperature reaches 280°C, take them out of the furnace and put them into the slow cooling pit to reach the temperature When it reaches 80°C, it is air-cooled to room temperature to obtain the required insulation brick. The composition of the insulation brick is shown in Table 1, and the thermal condu...

Embodiment 2

[0030] Insulation bricks are prepared by the following process:

[0031] 1) Mix potassium hexatitanate whiskers with a length of 60-80 μm, a diameter of 0.3-0.5 μm, and an aspect ratio of 150-200, alumina and cement with a particle size of 2-5 μm, and dry-roll for 20 minutes.

[0032] 2) Then add sodium carboxymethyl cellulose, water glass and water successively, continue rolling for 30 minutes, roll out, and shape the blank in the brick-making mold.

[0033] 3) Air-dry the above-mentioned insulating brick blanks for 72 hours, then bake them in the furnace at a heating rate of 40°C / h, heat them to a temperature of 600°C, keep them warm for 12 hours, and then cool them in the furnace. When it reaches 70°C, it is air-cooled to room temperature to obtain the required insulation brick. The composition of the insulation brick is shown in Table 1, and the thermal conductivity of the insulation brick is shown in Table 2.

Embodiment 3

[0035] Insulation bricks are prepared by the following process:

[0036] 1) Mix potassium hexatitanate whiskers with a length of 60-80 μm, a diameter of 0.3-0.5 μm, and an aspect ratio of 150-200, alumina and cement with a particle size of 2-5 μm, and dry-roll for 18 minutes.

[0037] 2) Then add sodium carboxymethyl cellulose, water glass and water successively, continue rolling for 28 minutes, roll out, and shape the blank in the brick-making mold.

[0038] 3) Air-dry the above-mentioned insulating brick blanks for 48 hours, then bake them in the furnace at a heating rate of 50°C / h, heat them to a temperature of 550°C, keep them warm for 13 hours, and then cool them in the furnace. When it reaches 90°C, it is air-cooled to room temperature to obtain the required insulation brick. The composition of the insulation brick is shown in Table 1, and the thermal conductivity of the insulation brick is shown in Table 2.

[0039] The composition of table 1 insulation brick (mass fr...

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Abstract

The invention discloses a potassium hexatitanate whisker heat insulating brick and a manufacturing method thereof and belongs to the technical field of heat insulating materials. The potassium hexatitanate whisker heat insulating brick comprises the following compositions in percentage by weight: 80-85% potassium hexatitanate whiskers, 7-12% alumina micro powder, 2-3% sodium silicate, 0.6-0.8% sodium carboxymethylcellulose, 1.5-1.8% cement and 3-4% water. The production method comprises the steps of: firstly mixing the potassium hexatitanate whiskers, alumina and cement, and conducting dry milling; then adding sodium carboxymethylcellulose, sodium silicate and water for continuous milling; forming and blanking in a brick making mold; and conducting natural withering for 48-72 hours, then roasting in a furnace at a temperature rising speed of 40-60 DEG C / h, heating to 500-600 DEG C, insulating for 12-15 hours and then cooling the furnace, discharging from the furnace for entering into a burial pit when the temperature is lower than 300 DEG C, and carrying out air cooling to the room temperature when the temperature is lower than 100 DEG C. The heat insulating brick has excellent heat insulating property, high heating efficiency and obvious energy-saving effect and excellent economic and social benefits, and can be popularized and applied.

Description

technical field [0001] The invention relates to a method for preparing a thermal insulation brick, in particular to a potassium hexatitanate whisker thermal insulation brick and a manufacturing method thereof, belonging to the technical field of thermal insulation materials. Background technique [0002] With the continuous improvement of my country's opening to the outside world and the continuous enhancement of energy conservation awareness, the demand for thermal insulation bricks of various enterprises is increasing, and the material of the products is increasingly developing towards high-purity and low-iron new varieties. At present, The thermal insulation bricks used in China are mainly high-alumina thermal insulation bricks, and my country has also formulated the national standard (GB / T3995) of "High-aluminum Thermal Insulation Refractory Bricks". In order to achieve the purpose of heat preservation and energy saving in traditional industrial furnaces, an insulation la...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B28/26C04B14/38
Inventor 符寒光蒋志强冯锡兰刘建伟魏永强
Owner BEIJING UNIV OF TECH