Organosilicone-nano compound modified polyurea corrosion-resisting coating for mechanical recovery well environment and preparation method for organosilicone-nano compound modified polyurea corrosion-resisting coating
A nano-composite, silicone technology, applied in coatings, anti-corrosion coatings, etc., to achieve excellent surface adsorption and concentration effects, large specific surface area, and rapid curing
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Embodiment 1
[0020] Preparation of component A: Weigh 49 parts of 4,4'-diphenylmethane diisocyanate, 31 parts of polyether polyol 220, and 20 parts of aminoethylaminopropyl polydimethylsiloxane; mix 4,4 '-Diphenylmethane diisocyanate was added to the reaction kettle, filled with nitrogen, stirred at a constant speed under a cold water bath at 10°C, and polyether polyol 220 and aminoethylaminopropyl polydimethylsiloxane were added dropwise to the kettle , keep warm while stirring; after the dropwise addition, keep warm at 70-90°C for 3 hours, take a sample to measure the content of free isocyanate groups to be 15.5%, cool and discharge to obtain component A;
[0021] Preparation of component R: weigh 10 parts T-5000, 28 copies D-2000, 30 parts of diethyltoluenediamine, 30 parts of nano powder, 1 part of Irganox1076 and 1 part of Tinuvin328; first mix nano powder, Irganox1076, Tinuvin328 and 5 parts T-5000, 14 copies D-2000, mix and grind until the grinding slurry with a fineness of 4...
Embodiment 2
[0024] Preparation of component A: Weigh 49 parts of 2,4'-diphenylmethane diisocyanate, 31 parts of polyether polyol 220, and 20 parts of aminoethylaminopropyl polydimethylsiloxane; mix 2,4 '-Diphenylmethane diisocyanate was added to the reaction kettle, filled with nitrogen, stirred at a constant speed under a cold water bath at 10°C, and polyether polyol 220 and aminoethylaminopropyl polydimethylsiloxane were added dropwise to the kettle , keep warm while stirring; after the dropwise addition, keep warm at 70-90°C for 3 hours, take a sample to measure the content of free isocyanate groups to be 15.5%, cool and discharge to obtain component A;
[0025] Preparation of component R: weigh 10 parts T-5000, 32 copies D-2000, 26 parts of diethyltoluenediamine, 20 parts of nano powder, 0.5 parts of Irganox1076 and 0.5 parts of Tinuvin328; first mix nano powder, Irganox1076, Tinuvin328 and 5 parts T-5000, 20 copies D-2000, mix and grind until the grinding slurry with a finenes...
Embodiment 3
[0028] Preparation of component A: Weigh 42 parts of MDI-50, 38 parts of polyether polyol 220, and 20 parts of aminoethylaminopropyl polydimethylsiloxane; add MDI-50 into the reaction kettle, fill with nitrogen , Stir at a constant speed in a cold water bath at 10°C, and add polyether polyol 220 and aminoethylaminopropyl polydimethylsiloxane dropwise to the kettle, and keep warm while stirring; After 3 hours of heat preservation, take a sample to measure the content of free isocyanate groups to be 15.5%, cool and discharge to obtain component A;
[0029] Preparation of component R: weigh 10 parts T-5000, 39 copies D-2000, 20 parts of diethyltoluenediamine, 30 parts of nano powder, 0.5 parts of Irganox1076 and 0.5 parts of Tinuvin328; first mix nano powder, Irganox1076, Tinuvin328 and 5 parts T-5000, 25 copies D-2000, mix and grind until the grinding slurry with a fineness of 35um is obtained; put the grinding slurry into the reaction kettle, add diethyltoluenediamine an...
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