Titanium surface casting modification method for reinforcing titanium-porcelain combination strength
A technology of bonding strength and modification, which is applied in the fields of pharmaceutical formulation, medical science, dentistry, etc., and can solve problems such as affecting the bonding of titanium porcelain and poor adhesion of oxide film
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[0030] Example 1
[0031] Take SiO 2 5g, grind and place in a porcelain cup for use; pour 35% hydrochloric acid and distilled water into the same beaker at a volume ratio of 1:1, mix well, and pour ethyl orthosilicate into another beaker, and acidify by the mixed hydrochloric acid The volume ratio of water to ethyl orthosilicate is 1:10, and then the acidified water with hydrochloric acid is slowly dropped into the ethyl orthosilicate beaker and stirred fully. The stirred mixture of ethyl orthosilicate and acidified water is continuously added with SiO while stirring 2 Powder (SiO 2 The amount of powder is 3.9-4 times the mass of tetraethyl orthosilicate). After all the addition is complete, continue to stir for 10-15 minutes to make SiO 2 The powder and the mixed liquid are fully reconciled. Coat the compatible inner embedding material on the side of the wax model that has been treated with affinity mist, and solidify at room temperature. Use the titanium professional embedding ...
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[0034] Example 2
[0035] Take SiO 2 Powder and 2μm particle size Al 2 O 3 Add 2.5g each of the powder to the ball mill tank, grind for 5 minutes until the two powders are fully mixed; pour 35% hydrochloric acid and distilled water into the same beaker at a volume ratio of 1:1, mix well, and pour aluminate into the other beaker. For calcium cement, the ratio of the mixed hydrochloric acid acidified water to calcium aluminate cement is 1:1, and then the hydrochloric acid acidified water is slowly dropped into the calcium aluminate cement, and fully stirred. The stirred calcium aluminate cement and acidified water mixture is continuously added with mixed SiO while stirring 2 Powder and Al 2 O 3 After adding all the powder and mixing powder, continue to stir for 10-15 minutes to make the powder and the mixed liquid fully mixed. Coat the compatible inner embedding material on the side of the wax model that has been treated with affinity mist, and solidify at room temperature. Use the...
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[0038] Example 3
[0039] Take SiO 2 Powder and ZrO 2 2.5g each of the powder, add it to the ball mill tank and grind for 5-10 minutes until the grinding is uniform; pour 35% hydrochloric acid and distilled water into the same beaker at a volume ratio of 1:1, mix well, and pour orthosilicic acid into another beaker. For ethyl ester, the volume ratio of the mixed hydrochloric acid acidified water and the ethyl orthosilicate is 1:10, and the hydrochloric acid acidified water is slowly dropped into the ethyl orthosilicate beaker, and the mixture is fully stirred. The stirred ethyl orthosilicate and acidified water mixture is continuously added with mixed SiO under stirring 2 Powder and ZrO 2 After all the powder is added, continue to stir for 10-15 minutes to make the powder and the mixed liquid fully mixed. Coat the compatible internal embedding material on the side of the wax model that has undergone the affinity mist treatment, and let it dry naturally at room temperature. Use th...
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