The application discloses a process for reducing the iron and
oxygen of
titanium sponge in the technical field of
titanium sponge production, which comprises the following steps: cleaning a reactor, assembling a
titanium infiltration frame, adding titanium
sponge for titanium infiltration, and assembling the reactor; putting the assembled reactor into a
distillation furnace, increasing the temperature of the furnace to a certain temperature, and then baking the reactor; increasing the temperature of the
distillation furnace to a specified temperature; rapidly increasing the temperature of the
distillation furnace after constant temperature, and simultaneously performing vacuumizing to perform first titanium infiltration; taking out the titanium infiltration device after furnace cooling, disassembling the reactor. Assembling the reactor,
leak detection after vacuumizing in a reduction furnace, and
argon filling. Adding a small amount of liquid
magnesium to assemble the reactor, increasing the temperature, and adding a small amount of
titanium tetrachloride to perform second titanium infiltration. The reduction, distillation and crushing obtain the titanium sponge. The process in the application can remove the water adsorbed on the surface of the reactor and the large cover after cleaning and the water adsorbed on the surface of titanium used for titanium infiltration, and avoids the influence of
oxygen and
hydrogen on the titanium infiltration process.