Process for production of polycarbonate resin pellets
A technology of polycarbonate resin and manufacturing method, applied in the direction of coating, etc., can solve the problem of sufficient cleanliness, and achieve the effect of no yellowing, less resin deterioration, and good appearance
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Embodiment 1)
[0161] Use intermeshing co-rotating twin-screw exhaust extruder (TEX30α manufactured by Japan Steel Works, barrel length 52.5D (D is the inner diameter of the barrel)), use image 3 The screw constitutes A.
[0162] Such as image 3 As shown, for the purpose of illustration, the extruder is divided into the same length from C 1 to C 15 from the hopper side to the die direction.
[0163] Screw composition A in such as image 3 Each area shown is structured as follows.
[0164] a) Melting zone: a forward screw with a length of 31.5D and a lead of 1.5D is connected.
[0165] b) Mixing zone: length 4.0D
[0166] Along the conveying direction, it includes a forward kneading element 1D, a reverse kneading element 0.5D and a forward kneading element 1.0D, an orthogonal kneading element 1.0D, and a reverse screw 0.5D. Among them, a liquid injection plug is installed in the C 10 barrel, and a plunger pump is used to add water.
[0167] c) Decompression zone: a positive screw with a length of 17....
Embodiment 2)
[0214] Except having used PC-2 instead of PC-1, it carried out similarly to Example 1, and manufactured pellets. The results are shown in Table 3.
Embodiment 3)
[0216] Except that the supply amount of nitrogen was increased and the oxygen concentration in the hopper chute was 0.1% by volume, pellets were produced in the same manner as in Example 1. The results are shown in Table 3.
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