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A kind of preparation method of para-aramid pulp reinforced polyimide fiber paper

A technology of para-aramid pulp and polyimide fiber is applied in the field of preparation of para-aramid pulp reinforced polyimide fiber paper, which can solve the problem of poor bonding force, poor connectivity of paper fibers, and paper strength. It can improve the strength, reduce the paper break and improve the dielectric properties.

Active Publication Date: 2015-08-19
陕西帕若德新材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, due to the characteristics of the polyimide fiber itself, the surface of the fiber is smooth, the fiber itself has high strength, and the beating phenomenon cannot occur, resulting in poor bonding between the fibers of the paper and poor connection between the fibers of the paper. Poor, paper strength is not high

Method used

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  • A kind of preparation method of para-aramid pulp reinforced polyimide fiber paper

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] Firstly, the polyimide chopped fibers are beaten for 30 minutes through a tank beater, so that the chopped fibers are fully dispersed and loosened to obtain polyimide fiber pulp; Defibrication and dispersion treatment is carried out inside, and the para-aramid pulp pulp is obtained by deflaking and dispersing until the degree of beating is 40°SR. The dry mass ratio of polyimide chopped fibers) is added to the polyimide fiber slurry to prepare polyimide fiber aramid pulp. In order to fully disperse the fibers and reduce flocculation, the polyimide Add PEO to the amine fiber aramid pulp, the addition amount is 0.005% (relative to the ratio of the absolute dry weight of the polyimide chopped fiber); then, the polyimide fiber aramid pulp enters the front flow system of the paper machine, Add styrene-butadiene latex and CPAM before the high-level box or headbox of the flow delivery system, and the addition amount is 20% (relative to the dry mass ratio of polyimide chopped fi...

Embodiment 2

[0021] Firstly, the polyimide chopped fibers are beaten for 10 minutes through a tank beater, so that the chopped fibers are fully dispersed and loosened to obtain a polyimide fiber slurry; the para-aramid pulp is placed in a tank beater Defibrication and dispersion treatment is carried out inside, and the para-aramid pulp pulp is obtained by deflaking and dispersing until the degree of beating is 60°SR. The dry mass ratio of polyimide chopped fibers) is added to the polyimide fiber slurry to prepare polyimide fiber aramid pulp. In order to fully disperse the fibers and reduce flocculation, the polyimide Add PEO to the amine fiber aramid pulp, and the addition amount is 1.0% (relative to the ratio of the absolute dry weight of the polyimide chopped fiber); then, the polyimide fiber aramid pulp enters the front flow system of the paper machine, Add styrene-butadiene latex and CPAM before the high-level box or headbox of the flow delivery system, and the addition amount is 0.05%...

Embodiment 3

[0023] Firstly, the polyimide chopped fibers are beaten for 120 minutes through a tank beater, so that the chopped fibers are fully dispersed and loosened to obtain polyimide fiber pulp; In the process of dissolving and dispersing, disentangling and dispersing until the beating degree is 20°SR to obtain para-aramid pulp pulp, the para-aramid pulp pulp is 20% (based on the absolute dry mass of para-aramid pulp, relative to The dry mass ratio of polyimide chopped fibers) is added to the polyimide fiber slurry to prepare polyimide fiber aramid pulp. In order to fully disperse the fibers and reduce flocculation, the polyimide Add PEO to the amine fiber aramid pulp, the addition amount is 0.15% (relative to the ratio of the absolute dry weight of the polyimide chopped fiber); then, the polyimide fiber aramid pulp enters the front flow system of the paper machine, Add styrene-butadiene latex and CPAM before the high-level box or headbox of the flow delivery system, and the addition ...

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Abstract

The present invention provides a para-aramid pulp enhanced polyimide fiber paper preparation method, which comprises: carrying out pulping on polyimide short-cut fibers through a groove type pulp beater to obtain a polyimide fiber pulp; carrying out an ease dispersion treatment on para-aramid pulp in the groove type pulp beater; adding the para-aramid pulp treated through ease dispersion to the polyimide fiber pulp, and mixing; after uniformly mixing, adding polyethylene oxide, styrene-butadiene latex and cation polyacrylamide; adopting a paper machine to carry out papermaking molding and drying to obtain base paper; and adopting a polyimide resin to immerse the base paper, and carrying out hot pressing through a hot pressing machine to obtain the polyimide fiber paper. According to the para-aramid pulp enhanced polyimide fiber paper preparation method, the para-aramid pulp is added to the polyimide fiber papermaking process so as to improve strength and papermaking of the polyimide fiber paper, reduce paper breaking during papermaking, improve speed and production efficiency of the paper machine, and improve a dielectric property of the product.

Description

technical field [0001] The invention belongs to the cross field of papermaking industry and material industry, and in particular relates to a preparation method of para-aramid pulp reinforced polyimide fiber paper. Background technique [0002] Polyimide fiber is a variety of high-performance fibers with high modulus, high strength, low water absorption, high and low temperature resistance, chemical corrosion resistance, hydrolysis resistance, radiation resistance, good electrical insulation and excellent heat resistance The characteristics of oxidation stability make it have broad application prospects in aerospace industry, electrical insulation, atomic energy industry, satellite, nuclear submarine and microelectronics industry. [0003] Composite materials made of polyimide fibers and their resins can be more widely used in high-tech industries, such as aviation cables, flexible printed cables, high-temperature insulating electrical appliances, aerospace rocket engine noz...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D21H13/26
Inventor 陆赵情花莉丁孟贤刘斌杨诚付饶孟育徐强
Owner 陕西帕若德新材料科技有限公司