Method for detecting content of iron in photovoltaic glass based on X-ray fluorescence energy spectrum
What is Al technical title?
Al technical title is built by PatSnap Al team. It summarizes the technical point description of the patent document.
A technology for photovoltaic glass and iron content, applied in the field of detection, can solve the shortage of standard samples for determination of iron content in photovoltaic glass, and achieve the effect of promoting quality improvement and stability, and standardizing the market
Active Publication Date: 2013-03-20
WUXI INSPECTION TESTING & CERTIFICATION INST
View PDF5 Cites 11 Cited by
Summary
Abstract
Description
Claims
Application Information
AI Technical Summary
This helps you quickly interpret patents by identifying the three key elements:
Problems solved by technology
Method used
Benefits of technology
Problems solved by technology
[0007] (1) Determination of calibration samples: use flame atomic absorption spectrometry to determine the iron content in representative photovol
Method used
the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more
Image
Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
Click on the blue label to locate the original text in one second.
Reading with bidirectional positioning of images and text.
Smart Image
Examples
Experimental program
Comparison scheme
Effect test
Embodiment 1
[0031] Example 1 Research on the Detection Method of Determination of Iron Content in Photovoltaic Glass by X-ray Fluorescence Spectroscopy (EDXRF)
[0032] 1. Instruments, samples and reagents
[0033] 1.1 Sample
[0034] 11 batches of photovoltaic glass from different sources: all collected by Wuxi Product Quality Supervision and Inspection Center;
[0035] 1.2 Reagents
[0036]Iron standard solution with a concentration of 1000μg / mL (GSB 04-1726-2004, value date August 2011, National Nonferrous Metals and Electronic Materials Analysis and Testing Center), hydrofluoric acid: electronic grade (Jiangyin Chemical Reagent Factory Co., Ltd. ), perchloric acid: analytically pure (Sinopharm Group Chemical Reagent Co., Ltd.), hydrochloric acid: electronic grade (Jiangyin Chemical Reagent Factory Co., Ltd.), boric acid: analytically pure (Shanghai Pilot Chemical Corporation);
[0037] 1.3 Instruments
[0038] Thermo QUANT'X X-ray fluorescence energy spectrometer (Thermo Electric ...
Embodiment 2
[0056] Example 2: Application research on the detection method of iron content in photovoltaic glass by X-ray fluorescence energy spectroscopy (EDXRF)
[0057] 1. Instruments, samples and reagents
[0058] 1.1 Sample
[0059] 29 batches of photovoltaic glass from different sources: all collected by Wuxi Product Quality Supervision and Inspection Center;
[0060] 1.2 Reagents
[0061] Iron standard solution with a concentration of 1000μg / mL (GSB 04-1726-2004, value date August 2011, National Nonferrous Metals and Electronic Materials Analysis and Testing Center), hydrofluoric acid: electronic grade (Jiangyin Chemical Reagent Factory Co., Ltd. ), perchloric acid: analytically pure (Sinopharm Group Chemical Reagent Co., Ltd.), hydrochloric acid: electronic grade (Jiangyin Chemical Reagent Factory Co., Ltd.), boric acid: analytically pure (Shanghai Pilot Chemical Corporation);
[0062] 1.3 Instruments
[0063] Thermo QUANT'X X-ray fluorescence energy spectrometer (Thermo Elect...
the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more
PUM
Login to view more
Abstract
The invention discloses a method for detecting content of iron in photovoltaic glass based on X-ray fluorescence energy spectrum, belonging to the technical field of detection. The method comprises the following steps of: selecting a representative photovoltaic glass sample, and manufacturing a calibration sample after the value of the iron content achieves constant by using a flame atomic absorption spectrometry, so that a problem that a standard sample in photovoltaic glass iron content measurement is in shortage is solved; measuring the calibration sample with constant photovoltaic glass iron content on an X-ray fluorescence energy disperse spectroscopy; establishing a calibration curve of the content of the iron in the photovoltaic glass, which is measured by adopting the X-ray fluorescence energy spectrum method; measuring the content of the sample in the photovoltaic glass sample by adopting the established calibration curve and the X-ray fluorescence energy disperse spectroscopy under a working condition the same as that in measuring the calibration sample. According to the method provided by the invention, the relative standard deviation (n =11) of the iron content measurement is between 4.5% and 9.0%, and the method is precise and reliable. The method is applied to analyzing a photovoltaic glass practical sample, the measured result is consistent with the analyzed result of the soda-lime-silica glass chemical analysis method of the national standard method GB/T1347-2008, and the working efficiency is more than 50 times that of the national standard method GB/T1347-2008, so that the requirements of quickly analyzing large-scale samples can be satisfied.
Description
technical field [0001] The invention relates to a detection method for determining the iron content in photovoltaic glass based on X-ray fluorescence energy spectroscopy (EDXRF), specifically an analysis method for rapidly and quantitatively determining the iron content in photovoltaic glass with an X-ray fluorescence energy spectroscopy instrument, which belongs to the detection method technology field. Background technique [0002] With the development of industry and the increase of human activities, human consumption of energy is increasing day by day, while underground non-renewable mineral energy is becoming increasingly scarce, and the contradiction between energy supply and demand is increasingly intensified. Energy issues have become one of the key issues affecting human survival and development. . Not only that, but the greenhouse gases produced by the burning of fossil energy accelerate the pace of global warming and cause various natural disasters to occur frequ...
Claims
the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more
Application Information
Patent Timeline
Application Date:The date an application was filed.
Publication Date:The date a patent or application was officially published.
First Publication Date:The earliest publication date of a patent with the same application number.
Issue Date:Publication date of the patent grant document.
PCT Entry Date:The Entry date of PCT National Phase.
Estimated Expiry Date:The statutory expiry date of a patent right according to the Patent Law, and it is the longest term of protection that the patent right can achieve without the termination of the patent right due to other reasons(Term extension factor has been taken into account ).
Invalid Date:Actual expiry date is based on effective date or publication date of legal transaction data of invalid patent.
Login to view more 
Login to view more