Erbium neodymium ion co-doped tellurium fluoride glass for emitting 2.7 microns of intermediate infrared light

A tellurium fluoride and neodymium ion technology is applied in the field of erbium neodymium ion co-doping tellurium fluoride glass to achieve the effects of excellent physical and chemical properties and high transmittance

Inactive Publication Date: 2013-04-03
SHANGHAI INST OF OPTICS & FINE MECHANICS CHINESE ACAD OF SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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At present, there are no reports at home and abroad on the reali

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  • Erbium neodymium ion co-doped tellurium fluoride glass for emitting 2.7 microns of intermediate infrared light
  • Erbium neodymium ion co-doped tellurium fluoride glass for emitting 2.7 microns of intermediate infrared light
  • Erbium neodymium ion co-doped tellurium fluoride glass for emitting 2.7 microns of intermediate infrared light

Examples

Experimental program
Comparison scheme
Effect test

Example Embodiment

[0024] Example 1 # :

[0025] Composition as shown in Table 1 # As shown, the specific preparation process is as follows:

[0026] According to 1 in Table 1 # The mole percentage of the glass composition, calculate the weight of each composition, weigh the raw materials and mix them evenly; put the mixture into a corundum crucible and melt it in a silicon carbide electric furnace at 1200°C for 15 minutes, and wait until the batch is completely melted Clarify for 15 minutes, pour the molten glass into a preheated mold; quickly move the glass into a muffle furnace that has been heated to 400°C, keep it for 10 hours, and then reduce to room temperature at a rate of 10°C / hour, and then cool completely Take out the glass sample.

[0027] The test results of the glass are as follows:

[0028] Take a few samples after annealing, grind them into fine powder with an agate mortar, and conduct differential thermal analysis test. The differential thermal curve of the 2.7μm infrared erbium neody...

Example Embodiment

[0030] Example 2 # :

[0031] Composition as shown in Table 1 2 # As shown, the specific preparation process is as follows:

[0032] According to 2 in Table 1 # The mole percentage of the glass composition, calculate the weight of each composition, weigh the raw materials and mix them evenly; put the mixture into a corundum crucible and melt it in a silicon carbide electric furnace at 1200°C for 15 minutes, and wait until the batch is completely melted Clarify for 15 minutes, pour the molten glass into a preheated mold; quickly move the glass into a muffle furnace that has been heated to 400°C, keep it for 10 hours, and then reduce to room temperature at a rate of 10°C / hour, and then cool completely Take out the glass sample.

[0033] The test results of the glass are as follows:

[0034] Take a few samples after annealing, grind them into fine powder with an agate mortar, and conduct differential thermal analysis test.

[0035] The annealed sample was processed into a 20×10×1.0mm gla...

Example Embodiment

[0036] Example 3 # :

[0037] Composition as shown in Table 1 in 3 # As shown, the specific preparation process is as follows:

[0038] According to 3 in Table 1 # The mole percentage of the glass composition, calculate the weight of each composition, weigh the raw materials and mix them evenly; put the mixture into a corundum crucible and melt it in a silicon carbide electric furnace at 1200°C for 15 minutes, and wait until the batch is completely melted Clarify for 15 minutes, pour the molten glass into a preheated mold; quickly move the glass into a muffle furnace that has been heated to 400°C, keep it for 10 hours, and then reduce to room temperature at a rate of 10°C / hour, and then cool completely Take out the glass sample.

[0039] The test results of the glass are as follows:

[0040] Take a few samples after annealing, grind them into fine powder with an agate mortar, and conduct differential thermal analysis test.

[0041] The annealed sample was processed into a 20×10×1.0 mm...

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Abstract

The invention discloses erbium neodymium ion co-doped tellurium fluoride glass for emitting 2.7 microns of intermediate infrared light. The glass comprises the following components in the range of mole percent: 55-65% of TeO2, 10-20% of GeO2, 0-20% of ZnO, 0-5% of Na2O, 0-20% of ZnF2, and 0-5% of NaF, and 0.5-1% of RE2O3, (RE is rare earth elements Er and Nd). The glass is prepared by a melting method of a corundum crucible and a silicon carbide rod electric furnace. The glass is transparent, not easy to devitrify, high in near infrared transmittance near 2708nm, and excellent in physical and chemical properties; the stability parameter delta T is greater than or equal to 140 DEG C; a strong 2.7 microns of intermediate infrared fluorescence can be obtained under pumping of a laser diode with 808nm of wavelength; and the glass is suitable for preparation and application of special glass doped with erbium ion for emitting 2.7 microns of intermediate infrared light and an optical fiber material.

Description

technical field [0001] The invention relates to a erbium neodymium ion co-doped tellurium fluoride glass emitting light at 2.7 μm in mid-infrared. Background technique [0002] Erbium ion-doped 2.7μm output solid-state lasers have attracted increasing attention in recent years because their wavelengths are very close to the absorption peak of water. field has important applications. Erbium ions are passed through 4 I 11 / 2 → 4 I 13 / 2 The transition achieves fluorescence emission near 2.7 μm, but due to the lower energy level 4 I 13 / 2 upper level 4 I 11 / 2 The long life, so can not get effective near 3μm wavelength fluorescence emission, usually by introducing other rare earth ions to reduce Er 3+ The lower energy level lifetime of the ions, resulting in an effective 2.7 μm fluorescence emission. Neodymium ions are rich in energy levels and compatible with erbium ions 4 I 13 / 2 The energy level is close to the abundant energy level, which is conducive to the lower en...

Claims

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Application Information

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IPC IPC(8): C03C4/12C03C3/253
Inventor 郭艳艳张军杰彭雅佩李明张丽艳胡丽丽
Owner SHANGHAI INST OF OPTICS & FINE MECHANICS CHINESE ACAD OF SCI
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