Preparation process of polyglycerol cement grinding aid
A cement grinding aid and preparation technology, which is applied in the fields of ether preparation, dehydration of hydroxyl-containing compounds to prepare ether, organic chemistry, etc., can solve the problems of low grinding efficiency, improve efficiency, improve grinding fineness and specific surface area , moderately priced effect
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Embodiment 1
[0019] ①. Preparation of polyglycerol cement grinding aid:
[0020] The polymerization of polyglycerol, add and reclaim glycerin 15%, NaOH 1%, kerosene 84% (all in weight ratio, the same below) in the reactor, pass N 2 Heating to 140°C under protection, keeping the reaction for 4 hours, calculating the average degree of polymerization n by measuring the refractive index of the reactants, and controlling the average degree of polymerization of polyglycerol to be 5.
[0021] The formula for calculating the average degree of polymerization is:
[0022] d 20 =nD t +0.00026(t-20)
[0023] Y=52480-34330nD 20
[0024] n=(56110×2-18Y) / (74Y-56110)
[0025] where: nD t is the refractive index at temperature t°C, nD 20 is the refractive index at a temperature of 20°C, Y is the hydroxyl value of polyglycerol, and n is the average degree of polymerization of polyglycerol.
[0026] ②. Preparation of polyglycerol cement grinding aid:
Embodiment 2
[0029] ①. Preparation of polyglycerol cement grinding aid:
[0030] For the polymerization of polyglycerol, 18% of recovered glycerin, 3% of NaOH and 79% of kerosene are added to the reactor, and the 2 Heating to 160°C under protection, keeping the temperature for 5 hours, calculating the average degree of polymerization n by measuring the refractive index of the reactants, and controlling the average degree of polymerization of polyglycerol to be 4.
[0031] ②. Preparation of polyglycerol cement grinding aid:
[0032] According to the weight ratio, 95% polyglycerin and 5% potassium aluminum sulfate can be mixed uniformly.
Embodiment 3
[0034] ①. Preparation of polyglycerol cement grinding aid:
[0035] For the polymerization of polyglycerol, 25% of recovered glycerin, 2% of NaOH and 73% of kerosene are added to the reactor, and N 2 Heating to 120°C under protection, keeping the reaction for 6 hours, calculating the average degree of polymerization n by measuring the refractive index of the reactants, and controlling the average degree of polymerization of polyglycerol to be 3.
[0036] ②. Preparation of polyglycerol cement grinding aid:
[0037] According to the weight ratio, 94% polyglycerin and 6% potassium aluminum sulfate can be mixed evenly.
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